Bis(4-azidophenyl)methanone

Base Information

Chemical Name:Bis(4-azidophenyl)methanone
CAS No.:17303-16-1
Molecular Formula:C13H8N6O
Molecular Weight:264.24200
Hs Code.:
DSSTox Substance ID:DTXSID80392394
Nikkaji Number:J951.388D
Wikidata:Q82190584

Synonyms:bis(4-azidophenyl)methanone;17303-16-1;4,4'-diazidobenzophenone;SCHEMBL13882615;DTXSID80392394;STK367741;AKOS005444943;bis[4-(1H-triaziren-1-yl)phenyl]methanone;AG-690/11763435

Suppliers and Price of Bis(4-azidophenyl)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of Bis(4-azidophenyl)methanone

Chemical Property:

PSA：116.57000
LogP:3.70672
XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:264.07595890
Heavy Atom Count:20
Complexity:396

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C(=O)C2=CC=C(C=C2)N=[N+]=[N-])N=[N+]=[N-]

Technology Process of Bis(4-azidophenyl)methanone

There total 6 articles about Bis(4-azidophenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 611-99-4
4,4'-Dihydroxybenzophenone

: 17303-16-1
bis(4-azidophenyl)methanone

Guidance literature:: With diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; for 16h; Reflux;
DOI:10.1016/j.tetlet.2019.151493

Reference yield:

: 3740-55-4
2,2-bis(4-nitrophenyl)ethanoic acid

: 17303-16-1
bis(4-azidophenyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1: CrO₃, glacial CH₃COOH / 18 h / Heating

2: 66 percent / SnCl₂*2H₂O / ethanol / 0.75 h / 70 °C

3: 1.) aq. HCl, NaMO₂, 2.) NaN₃ / 1.) 0 deg C to 5 deg C, 1 h, 2.) 15 min

With chromium(VI) oxide; hydrogenchloride; sodium azide; acetic acid; tin(ll) chloride; In ethanol;

Reference yield:

: 3469-00-9
methyl 2,2-diphenylacetate

: 17303-16-1
bis(4-azidophenyl)methanone

Guidance literature:: Multi-step reaction with 5 steps

1: 16 percent / fuming HNO₃ / 4.5 h / Ambient temperature

2: CH₃COOH, H₂SO₄ / 18 h / Heating

3: CrO₃, glacial CH₃COOH / 18 h / Heating

4: 66 percent / SnCl₂*2H₂O / ethanol / 0.75 h / 70 °C

5: 1.) aq. HCl, NaMO₂, 2.) NaN₃ / 1.) 0 deg C to 5 deg C, 1 h, 2.) 15 min

With chromium(VI) oxide; hydrogenchloride; sodium azide; sulfuric acid; nitric acid; acetic acid; tin(ll) chloride; In ethanol;