Benzyl-O-(2,3,4,6-tetra-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->3)-O-<(3,4,6-tri-O-acetyl-2-azido-2-desoxy-β-D-mannopyranosyl)-(1->4)>-2-O-acetyl-α-L-rhamnopyranosid

Base Information

• Chemical Name: Benzyl-O-(2,3,4,6-tetra-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->3)-O-<(3,4,6-tri-O-acetyl-2-azido-2-desoxy-β-D-mannopyranosyl)-(1->4)>-2-O-acetyl-α-L-rhamnopyranosid
• CAS No.: 101981-36-6
• Molecular Formula: C₈₈H₉₇N₃O₂₃
• Molecular Weight: 1578.63
• Mol file: 101981-36-6.mol

Synonyms:

Chemical Property of Benzyl-O-(2,3,4,6-tetra-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->3)-O-<(3,4,6-tri-O-acetyl-2-azido-2-desoxy-β-D-mannopyranosyl)-(1->4)>-2-O-acetyl-α-L-rhamnopyranosid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzyl-O-(2,3,4,6-tetra-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->3)-O-<(3,4,6-tri-O-acetyl-2-azido-2-desoxy-β-D-mannopyranosyl)-(1->4)>-2-O-acetyl-α-L-rhamnopyranosid

There total 1 articles about Benzyl-O-(2,3,4,6-tetra-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->3)-O-<(3,4,6-tri-O-acetyl-2-azido-2-desoxy-β-D-mannopyranosyl)-(1->4)>-2-O-acetyl-α-L-rhamnopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetic anhydride (108-24-7) + 2,3,6-Tri-O-<α,α-D2>benzyl-4-O-(2,3,4,6-tetra-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-α-D-glucopyranosylchlorid (101981-34-4) + Benzyl-2-O-acetyl-4-O-(3,4,6-tri-O-acetyl-2-azido-2-desoxy-β-D-mannopyranosyl)-α-L-rhamnopyranosid (101981-22-0) → Benzyl-O-(2,3,4,6-tetra-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-<α,α-D2>benzyl-β-D-glucopyranosyl)-(1->3)-O-<(3,4,6-tri-O-acetyl-2-azido-2-desoxy-β-D-mannopyranosyl)-(1->4)>-2-O-acetyl-α-L-rhamnopyranosid (102045-75-0) + Benzyl-O-(2,3,4,6-tetra-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->3)-O-<(3,4,6-tri-O-acetyl-2-azido-2-desoxy-β-D-mannopyranosyl)-(1->4)>-2-O-acetyl-α-L-rhamnopyranosid (101981-36-6)

Guidance literature:

With molecular sieve; silver trifluoromethanesulfonate; tetramethylurea; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, room temp., 4 h, 2.) pyridine, room temp., 6 h;

Reference yield:

acetic anhydride (108-24-7) + Benzyl-O-(2,3,4,6-tetra-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->3)-O-<(3,4,6-tri-O-acetyl-2-azido-2-desoxy-β-D-mannopyranosyl)-(1->4)>-2-O-acetyl-α-L-rhamnopyranosid (101981-36-6) → Benzyl-O-(2,3,4,6-tetra-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-<α,α-D2>benzyl-β-D-glucopyranosyl)-(1->3)-O-<(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-mannopyranosyl)-(1->4)>-2-O-acetyl-α-L-rhamnopyranosid (101981-37-7)

Guidance literature:

With hydrogen sulfide; triethylamine; Yield given. Multistep reaction; 1.) pyridine, water, room temp., 30 h, 2.) pyridine, 0 deg C, 6 h;

upstream raw materials:

acetic anhydride

2,3,6-Tri-O-<α,α-D2>benzyl-4-O-(2,3,4,6-tetra-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-α-D-glucopyranosylchlorid

Benzyl-2-O-acetyl-4-O-(3,4,6-tri-O-acetyl-2-azido-2-desoxy-β-D-mannopyranosyl)-α-L-rhamnopyranosid

Downstream raw materials:

Benzyl-O-(2,3,4,6-tetra-O-<α,α-D2>benzyl-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-<α,α-D2>benzyl-β-D-glucopyranosyl)-(1->3)-O-<(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-mannopyranosyl)-(1->4)>-2-O-acetyl-α-L-rhamnopyranosid