Benzoic acid, 2-[(2-methoxyphenyl)amino]-4-nitro-

Base Information

Chemical Name:Benzoic acid, 2-[(2-methoxyphenyl)amino]-4-nitro-
CAS No.:1744-93-0
Molecular Formula:C14H12N2O5
Molecular Weight:288.26
Hs Code.:
DSSTox Substance ID:DTXSID20445499
Wikidata:Q82263931

Synonyms:1744-93-0;Benzoic acid, 2-[(2-methoxyphenyl)amino]-4-nitro-;2-(2-methoxyanilino)-4-nitrobenzoic acid;2-[(2-METHOXYPHENYL)AMINO]-4-NITROBENZOIC ACID;DTXSID20445499;AKOS013363948;SS-5209

Suppliers and Price of Benzoic acid, 2-[(2-methoxyphenyl)amino]-4-nitro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzoic acid, 2-[(2-methoxyphenyl)amino]-4-nitro-

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:288.07462149
Heavy Atom Count:21
Complexity:384

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC=C1NC2=C(C=CC(=C2)[N+](=O)[O-])C(=O)O

Technology Process of Benzoic acid, 2-[(2-methoxyphenyl)amino]-4-nitro-

There total 1 articles about Benzoic acid, 2-[(2-methoxyphenyl)amino]-4-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 99-60-5
2-chloro-4-nitrobenzoic acid

: 90-04-0
2-methoxy-phenylamine

: 1744-93-0
2-(2-methoxyanilino)-4-nitrobenzoic acid

Guidance literature:: With pyridine; copper; potassium carbonate; In pentan-1-ol; for 5h; Heating;
DOI:10.1016/j.tet.2004.05.013

Reference yield: 63.0%

: 1744-93-0
2-(2-methoxyanilino)-4-nitrobenzoic acid

: 79-19-6
thiosemicarbazide

: 195370-49-1
C₁₅H₁₅N₅O₄S

Guidance literature:: 2-(2-methoxyanilino)-4-nitrobenzoic acid; With thionyl chloride; In benzene; for 0.5h; Heating;

thiosemicarbazide; In 1,4-dioxane; for 0.0833333h; Heating;
DOI:10.1007/BF02218832

Reference yield:

: 1744-93-0
2-(2-methoxyanilino)-4-nitrobenzoic acid

: 9-(4-chlorophenylhydrazino)-4-methoxy-6-nitroacridine

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / conc. H₂SO₄ / 4 h / 100 °C

2: SOCl₂, DMF / 2 h / Heating

3: 36 percent / TEA / dimethylformamide / 1) r.t., 2 h, 2) reflux, 16 h

With thionyl chloride; TEA; sulfuric acid; N,N-dimethyl-formamide; In N,N-dimethyl-formamide;
DOI:10.1002/ardp.19973300903