1H-Indole, 1-(4-bromophenyl)-

Base Information

• Chemical Name: 1H-Indole, 1-(4-bromophenyl)-
• CAS No.: 174621-52-4
• Molecular Formula: C14H10BrN
• Molecular Weight: 272.144

Synonyms:1-(4-Bromophenyl)-1H-indole;N-p-bromophenylindole;1-(4-bromophenyl)indole;N-(4-bromophenyl)-1H-indole;N-p-bromophenyl indole;N-(4-bromophenyl)indole;1-(4-Bromo-phenyl)-1H-indole;

Chemical Property of 1H-Indole, 1-(4-bromophenyl)-

Chemical Property:

• Melting Point: 64 - 65 °C
• Boiling Point: 370.8±34.0 °C(Predicted)
• PSA: 4.93000
• Density: 1.38±0.1 g/cm3(Predicted)
• LogP: 4.39300

Purity/Quality:

95% ^*data from raw suppliers

1-(4-Bromo-phenyl)-1H-indole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1H-Indole, 1-(4-bromophenyl)-

There total 6 articles about 1H-Indole, 1-(4-bromophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

indole (120-72-9) + 1,4-bromoiodobenzene (589-87-7) → N-(4-bromophenyl)-1H-indole (174621-52-4)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 110 ℃; for 2h;

DOI:10.1002/aoc.3296

Reference yield: 87.0%

indole (120-72-9) + 1-Bromo-4-fluorobenzene (460-00-4) → N-(4-bromophenyl)-1H-indole (174621-52-4)

Guidance literature:

With potassium phosphate; In N,N-dimethyl-formamide; at 190 ℃; for 1h; Microwave irradiation;

DOI:10.1002/anie.201202149

Reference yield: 83.0%

indole (120-72-9) + bis(4-bromophenyl)iodonium bromide (65826-67-7) → N-(4-bromophenyl)-1H-indole (174621-52-4)

Guidance literature:

With sodium hydride; 1-butyl-3-methylimidazolium Tetrafluoroborate; at 40 ℃;

upstream raw materials:

indole

1-Bromo-4-fluorobenzene

bis(4-bromophenyl)iodonium bromide

1,4-bromoiodobenzene

Downstream raw materials:

4'-Indol-1-yl-biphenyl-4-carbaldehyde

(-)-ethyl (R)-2-(1-(4-bromophenyl)-1H-indol-3-yl)hexanoate

1-(4-{10-[4-(1H-indol-1-yl)phenyl]-4,7,13,16-tetraphenylcyclooctadeca-1,2,3,7,8,9,13,14,15-nonaen-5,11,17-triyn-1-yl}phenyl)-1H-indole (p-bis(4-(indol-1-yl)phenyl)-tetra-phenyl-carbobenzene)

1,10-bis[4-(1H-indol-1-yl)phenyl]-4,7,13,16-tetramethoxy-4,7,13,16-tetraphenylcyclooctadeca-2,5,8,11,14,17-hexayne-1,10-diol

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