[(4-methylphenyl)imino]diethane-2,1-diyl bis(4-methylbenzenesulfonate)

Base Information

• Chemical Name: [(4-methylphenyl)imino]diethane-2,1-diyl bis(4-methylbenzenesulfonate)
• CAS No.: 15314-38-2
• Molecular Formula: C25H29 N O6 S2
• Molecular Weight: 503.6309
• Mol file: 15314-38-2.mol

Synonyms:Ethanol,2,2'-(p-tolylimino)di-, di-p-toluenesulfonate (ester) (8CI); N-(4-Methylphenyl)diethanolamineditosylate; NSC 82273

Chemical Property of [(4-methylphenyl)imino]diethane-2,1-diyl bis(4-methylbenzenesulfonate)

Chemical Property:

• Vapor Pressure: 2.85E-18mmHg at 25°C
• Boiling Point: 678.6°C at 760 mmHg
• Flash Point: 364.2°C
• Density: 1.277g/cm³

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [(4-methylphenyl)imino]diethane-2,1-diyl bis(4-methylbenzenesulfonate)

There total 1 articles about [(4-methylphenyl)imino]diethane-2,1-diyl bis(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-bis-(2-hydroxyethyl)-P-toluidine (3077-12-1) + p-toluenesulfonyl chloride (98-59-9) → C25H29NO6S2 (15314-38-2)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃;

DOI:10.1016/j.bmcl.2010.02.071

Reference yield:

C25H29NO6S2 (15314-38-2) + (S)-amino-3-<4-<2-(5-methyl-2-phenyloxazol-4-yl)ethoxy>phenyl>propionic acid methyl ester (196811-04-8) → C33H37N3O4

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydrogencarbonate; at 140 ℃;

DOI:10.1016/j.bmcl.2010.02.071

upstream raw materials:

N,N-bis-(2-hydroxyethyl)-P-toluidine

p-toluenesulfonyl chloride

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