Ru(C₁₃H₁₂N₄S)(CH₃OH)Cl₂

Base Information

Chemical Name:Ru(C₁₃H₁₂N₄S)(CH₃OH)Cl₂
CAS No.:125955-58-0
Molecular Formula:C₁₄H₁₆Cl₂N₄ORuS
Molecular Weight:460.349
Hs Code.:

Ru(C<sub>13</sub>H<sub>12</sub>N<sub>4</sub>S)(CH<sub>3</sub>OH)Cl<sub>2</sub>

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Chemical Property of Ru(C₁₃H₁₂N₄S)(CH₃OH)Cl₂

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Technology Process of Ru(C₁₃H₁₂N₄S)(CH₃OH)Cl₂

There total 1 articles about Ru(C₁₃H₁₂N₄S)(CH₃OH)Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6839-89-0
pyridine-2-formaldehyde N⁴-phenyl thiosemicarbazone

: 10049-08-8,63767-78-2
ruthenium(III)chloride

: Ru₂(C₁₃H₁₁N₄S)(H₂O)Cl₄

: 125955-58-0
Ru(C₁₃H₁₂N₄S)(CH₃OH)Cl₂

Guidance literature:: In methanol; addn. of soln. of the ligand in MeOH to RuCl3 in MeOH (3-4 h, stirred), stirred (3 h); filtration, washed (MeOH, several times), dried over fused CaCl2: gives Ru2-complex; evapn. of filtrate to dryness, washed (H2O), recrystn. (MeOH); elem. anal.;
DOI:10.1016/S0020-1693(00)83458-1

Reference yield:

: 125955-58-0
Ru(C₁₃H₁₂N₄S)(CH₃OH)Cl₂

: Ru⁽²⁺⁾*C₁₃H₁₂N₄S*HN(C₆H₄(CH₃))CSNNH₂^(1-)*Cl^(1-)*0.5O(C₂H₅)2={Ru(C₁₃H₁₂N₄S)(HN(C₆H₄(CH₃))CSNNH₂)}Cl*0.5O(C₂H₅)2

Guidance literature:: In methanol; addn. of bipyridyl to soln. of Ru-complex in MeOH, stirred (18 h); filtration, evapn. of filtrate to dryness on a hot plate, kept (sulfuric acid desiccator, 2 d), several times triturated with acetone, recrystn. (CH2Cl2 with a small volume of methanol); elem. anal.;
DOI:10.1016/S0020-1693(00)83458-1