2-[(4,6-Dimethylpyrimidin-2-yl)disulfanyl]-4,6-dimethylpyrimidine

Base Information

Chemical Name:2-[(4,6-Dimethylpyrimidin-2-yl)disulfanyl]-4,6-dimethylpyrimidine
CAS No.:17624-79-2
Molecular Formula:C12H14N4S2
Molecular Weight:278.402
Hs Code.:
DSSTox Substance ID:DTXSID20353085
Nikkaji Number:J680.206K
Wikidata:Q82130535
ChEMBL ID:CHEMBL1548507

Synonyms:17624-79-2;Pyrimidine, 2,2'-dithiobis[4,6-dimethyl-;MLS001183558;SMR000502009;2-[(4,6-dimethylpyrimidin-2-yl)disulfanyl]-4,6-dimethylpyrimidine;HMS2817L07;cid_736679;SCHEMBL7074739;CHEMBL1548507;BDBM60854;DTXSID20353085;STK089091;AKOS003212495;1,2-Bis(4,6-dimethylpyrimidin-2-yl)disulfane;2,2'-disulfanediylbis(4,6-dimethylpyrimidine);2-[(4,6-dimethyl-2-pyrimidinyl)disulfanyl]-4,6-dimethylpyrimidine;2-[(4,6-dimethylpyrimidin-2-yl)disulfanyl]-4,6-dimethyl-pyrimidine

Suppliers and Price of 2-[(4,6-Dimethylpyrimidin-2-yl)disulfanyl]-4,6-dimethylpyrimidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(4,6-Dimethylpyrimidin-2-yl)disulfanyl]-4,6-dimethylpyrimidine

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:278.06598881
Heavy Atom Count:18
Complexity:221

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=NC(=N1)SSC2=NC(=CC(=N2)C)C)C

Technology Process of 2-[(4,6-Dimethylpyrimidin-2-yl)disulfanyl]-4,6-dimethylpyrimidine

There total 1 articles about 2-[(4,6-Dimethylpyrimidin-2-yl)disulfanyl]-4,6-dimethylpyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 123-56-8,89963-74-6
Succinimide

: 22325-27-5,131321-42-1
4,6-dimethyl-2-meraptopyrimidine

: 1060674-84-1
1-((4,6-dimethylpyrimidin-2-yl)thio)pyrrolidine-2,5-dione

: 17624-79-2
1,2-bis(4,6-dimethylpyrimidin-2-yl)disulfane

Guidance literature:: 4,6-dimethyl-2-meraptopyrimidine; With sulfuryl dichloride; triethylamine; In dichloromethane; at 0 - 20 ℃;

Succinimide; With triethylamine; In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1021/ol4036209

Reference yield: 70.0%

: 20332-49-4,14741-36-7
tricarbonylbis(triphenylphosphine)ruthenium⁽⁰⁾

: 17624-79-2
1,2-bis(4,6-dimethylpyrimidin-2-yl)disulfane

: carbonylbis(4,6-dimethylpyrimidine-2-thiolato)(triphenylphosphine)ruthenium

: carbonylbis(4,6-dimethylpyrimidine-2-thiolato)(triphenylphosphine)ruthenium

: dicarbonylbis(4,6-dimethylpyrimidine-2-thiolato)(triphenylphosphine)ruthenium

Guidance literature:: In toluene; heating the Ru-compd. to reflux, rapid addn. of the disulphide, heating under reflux for 8 min, rapid cooling (water ca. 15°C); evapg. to dryness under reduced pressure, recrystn. from CH2Cl2-diethyl ether, filtration, washing with light petroleum and diethyl ether, drying in vac., elem. anal.;
DOI:10.1016/S0020-1693(00)83232-6

Reference yield: 33.0%

: 15318-31-7,14871-41-1,59246-46-7
bis(triphenylphosphine)iridium(I) carbonyl chloride

: 17624-79-2
1,2-bis(4,6-dimethylpyrimidin-2-yl)disulfane

: 127312-85-0
carbonylchlorohydrido(4,6-dimethylpyrimidine-2-thiolato)bis(triphenylphosphine)iridium

Guidance literature:: With triphenylphosphine; In benzene; stirring at ambient temp. for 3 h, addn. of light petroleum, pptn.; filtration, washing with light petroleum and diethyl ether, drying in vac., elem. anal.;
DOI:10.1016/S0020-1693(00)83232-6