Carbamic acid, cyclohexyl-, butyl ester

Base Information

• Chemical Name: Carbamic acid, cyclohexyl-, butyl ester
• CAS No.: 17671-80-6
• Molecular Formula: C11H21NO2
• Molecular Weight: 199.293
• Mol file: 17671-80-6.mol

Synonyms:

Chemical Property of Carbamic acid, cyclohexyl-, butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbamic acid, cyclohexyl-, butyl ester

There total 21 articles about Carbamic acid, cyclohexyl-, butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

cyclohexylamine (108-91-8,157973-60-9) + carbonochloridic acid, butyl ester (592-34-7) → butyl N-cyclohexylcarbamate (17671-80-6)

Guidance literature:

In benzene; Heating;

Reference yield: 92.0%

cyclohexylamine (108-91-8,157973-60-9) + (1-butyl)-(-4-oxy-phenylene) carbonate (81577-19-7) → butyl N-cyclohexylcarbamate (17671-80-6) + hydroquinone (123-31-9,8027-02-9)

Guidance literature:

With N,N-dimethyl-formamide;

Reference yield: 92.0%

1,3-Dicyclohexylurea (2387-23-7) + butan-1-ol (71-36-3) → butyl N-cyclohexylcarbamate (17671-80-6)

Guidance literature:

4.0 wt. % LaO_x, 2.0 wt. % CeO_y, 3.0 wt. % TiO₂; at 210 ℃; for 10h; under 3750.38 Torr; Product distribution / selectivity; sealed reactor;

upstream raw materials:

tert-Butyl peroxybenzoate

dicyclohexyl-carbodiimide

butan-1-ol

butyl phenyl carbonate

Refernces

• 1、 Ogbu, Ikechukwu Martin,Lusseau, Jonathan,Kurtay, Gülbin,Robert, Frédéric,Landais, Yannick. "Urethanes synthesis from oxamic acids under electrochemical conditions". . p. 12226 - 12229. Retrieved 2020/10/26.
• 2、 Senadi, Gopal Chandru,Mutra, Mohana Reddy,Lu, Ting-Yi,Wang, Jeh-Jeng. "Oximes as reusable templates for the synthesis of ureas and carbamates by an: In situ generation of carbamoyl oximes". . p. 4272 - 4277. Retrieved 2017/09/28.