4,5-Dibutoxy-1,2-benzenediamine

Base Information

Chemical Name:4,5-Dibutoxy-1,2-benzenediamine
CAS No.:1770-37-2
Molecular Formula:C14H24N2O2
Molecular Weight:252.357
Hs Code.:
DSSTox Substance ID:DTXSID301303690
Nikkaji Number:J1.864.812A

Synonyms:4,5-Dibutoxy-1,2-benzenediamine;DTXSID301303690;1770-37-2

Suppliers and Price of 4,5-Dibutoxy-1,2-benzenediamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4,5-Dibutoxy-1,2-benzenediamine

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:252.183778013
Heavy Atom Count:18
Complexity:192

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCCCOC1=C(C=C(C(=C1)N)N)OCCCC

Technology Process of 4,5-Dibutoxy-1,2-benzenediamine

There total 5 articles about 4,5-Dibutoxy-1,2-benzenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20367-37-7
1,2-dibutoxy-4,5-dinitrobenzene

: 1770-37-2
1,2,-diamino-4,5-dibutoxybenzene

Guidance literature:: With hydrogenchloride; tin;

Reference yield:

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 1770-37-2
1,2,-diamino-4,5-dibutoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / acetone / Heating

2: HNO₃; AcOH / CH₂Cl₂

3: hydrogen / Pd/C / ethanol

With hydrogen; nitric acid; potassium carbonate; acetic acid; palladium on activated charcoal; In ethanol; dichloromethane; acetone;
DOI:10.1016/S0040-4039(02)02862-9

Reference yield:

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 1770-37-2
1,2,-diamino-4,5-dibutoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / potassium carbonate / acetone

2: 63 percent / 70percent HNO₃ / 80 °C

3: H₂ / Pd/C / ethyl acetate

With hydrogen; nitric acid; potassium carbonate; palladium on activated charcoal; In ethyl acetate; acetone;
DOI:10.1016/0040-4039(95)01562-V