(3-Bromopropoxy)(tert-butyl)diphenylsilane

Base Information

Chemical Name:(3-Bromopropoxy)(tert-butyl)diphenylsilane
CAS No.:177338-13-5
Molecular Formula:C19H25BrOSi
Molecular Weight:377.396
Hs Code.:
European Community (EC) Number:961-988-5

Synonyms:(3-Bromopropoxy)(tert-butyl)diphenylsilane;177338-13-5;SCHEMBL2986951;XEJWSBVHJKWEKC-UHFFFAOYSA-N;3-bromopropoxy-tert-butyl-diphenylsilane;3-(t-butyldiphenylsilyloxy)propyl bromide;EN300-33251084;A1-30840

Suppliers and Price of (3-Bromopropoxy)(tert-butyl)diphenylsilane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of (3-Bromopropoxy)(tert-butyl)diphenylsilane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:7
Exact Mass:376.08580
Heavy Atom Count:22
Complexity:296

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)[Si](C1=CC=CC=C1)(C2=CC=CC=C2)OCCCBr

Technology Process of (3-Bromopropoxy)(tert-butyl)diphenylsilane

There total 2 articles about (3-Bromopropoxy)(tert-butyl)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 627-18-9
1-bromo-3-propanol

: 177338-13-5
3-(tert-butyldiphenylsilyloxy)propyl bromide

Guidance literature:: With 1H-imidazole; In dichloromethane; for 21h; Inert atmosphere;
DOI:10.1016/j.tet.2009.03.031

Reference yield: 93.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 627-18-9
1-bromo-3-propanol

: 177338-13-5
3-(tert-butyldiphenylsilyloxy)propyl bromide

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1002/chem.201202553

Reference yield: 100.0%

: 6089-04-9
3-(tetrahydropyran-2'-yloxy)propyne

: 177338-13-5
3-(tert-butyldiphenylsilyloxy)propyl bromide

: 1-(tetrahydropyran-2-yloxy)-6-tert-butyldiphenylsilyloxyhex-2-yne

Guidance literature:: 3-(tetrahydropyran-2'-yloxy)propyne; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h; Inert atmosphere;

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; In tetrahydrofuran; hexane; at 0 ℃; for 0.166667h; Inert atmosphere;

3-(tert-butyldiphenylsilyloxy)propyl bromide; In tetrahydrofuran; hexane; at 0 ℃; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2009.03.031