6-PHENYLHEXYLAMINE

Base Information

• Chemical Name: 6-PHENYLHEXYLAMINE
• CAS No.: 17734-20-2
• Molecular Formula: C12H19N
• Molecular Weight: 177.29
• Hs Code.: 2921499090
• Mol file: 17734-20-2.mol

Synonyms:6-phenyl-1-hexylamine;6-phenylhexyl amine;Benzenehexanamine;Phenylhexylamine;16-Amino-1-n-hexyl-benzol;1-amino-6-phenylhexane;Hexylamine,6-phenyl;

Chemical Property of 6-PHENYLHEXYLAMINE

Chemical Property:

• PSA: 26.02000
• LogP: 3.44850
• Solubility.: Dichloromethane, Ethyl Acetate, Methanol

Purity/Quality:

98% ^*data from raw suppliers

6-Phenylhexylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 6-Phenylhexylamine_x000D_Discontinued see: P329051 (cas# 17734-20-2) is a compound useful in organic synthesis.

Technology Process of 6-PHENYLHEXYLAMINE

There total 11 articles about 6-PHENYLHEXYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.53%

2-(6-phenylhexyl)-1,3-dihydro-1,3-dioxo-2H-isoindole (138619-78-0) → 6-phenylhexylamine (17734-20-2)

Guidance literature:

2-(6-phenylhexyl)-1,3-dihydro-1,3-dioxo-2H-isoindole; With hydrazine hydrate; In ethanol; for 5h; Reflux;

With hydrogenchloride; In ethanol; water; for 0.5h; Reflux;

DOI:10.1021/acs.jmedchem.6b00609

Reference yield: 90.0%

6-phenyl-1-hexanol (2430-16-2) → 6-phenylhexylamine (17734-20-2)

Guidance literature:

6-phenyl-1-hexanol; In dichloromethane; cooling;

With dibenzyl azodicarboxylate; In dichloromethane; cooling;

With trifluoroacetic acid; In dichloromethane; Further stages.;

DOI:10.1016/j.tetlet.2007.09.034

Reference yield:

6-phenyl-hex-2-ynylamine → 6-phenylhexylamine (17734-20-2) + (Z)-6-Phenyl-hex-2-enylamine + (E)-6-Phenyl-hex-2-enylamine

Guidance literature:

With diazoacetic acid ethyl ester; hydrogen; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

DOI:10.1021/jo015514a

upstream raw materials:

6-phenylhexanenitrile

2-(6-phenylhexyl)-1,3-dihydro-1,3-dioxo-2H-isoindole

6-phenyl-1-hexanol

(6-bromohexyl)benzene

Downstream raw materials:

N-Acetyl-6-phenylhexylamin

2'-(2-hydroxy-ethoxy)-4''-methoxy-3-trifluoromethyl-[1,1';3',1'']terphenyl-5'-carboxylic acid (6-phenyl-hexyl)-amide

2'-(2-hydroxy-ethoxy)-3,3''-bis-trifluoromethyl-[1,1';3',1'']terphenyl-5'-carboxylic acid (6-phenyl-hexyl)-amide

5-Acetylamino-2-(6-phenylhexyl-amino)-tetralinehydrochloride

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