5-(2-oxopropyl)-5-(prop-2-en-1-yl)pyrimidine-2,4,6(1H,3H,5H)-trione

Base Information

• Chemical Name: 5-(2-oxopropyl)-5-(prop-2-en-1-yl)pyrimidine-2,4,6(1H,3H,5H)-trione
• CAS No.: 21248-32-8
• Molecular Formula: C10H12 N2 O4
• Molecular Weight: 224.2133
• Mol file: 21248-32-8.mol

Synonyms:2,4,6(1H,3H,5H)-Pyrimidinetrione,5-(2-oxopropyl)-5-(2-propenyl)- (9CI); Barbituric acid, 5-acetonyl-5-allyl-(6CI,8CI); 5-Allyl-5-acetonylbarbituric acid

Chemical Property of 5-(2-oxopropyl)-5-(prop-2-en-1-yl)pyrimidine-2,4,6(1H,3H,5H)-trione

Chemical Property:

• Density: 1.2g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-(2-oxopropyl)-5-(prop-2-en-1-yl)pyrimidine-2,4,6(1H,3H,5H)-trione

There total 7 articles about 5-(2-oxopropyl)-5-(prop-2-en-1-yl)pyrimidine-2,4,6(1H,3H,5H)-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(2-oxopropyl)perhydropyrimidine-2,4,6-trione (165903-83-3) + allyl bromide (106-95-6) → 5-Acetonyl-5-allyl-barbitursaeure (21248-32-8)

Guidance literature:

With water;

Reference yield:

chloroacetone (78-95-5) + 5-allyl-pyrimidine-2,4,6-trione (2565-43-7) → 5-Acetonyl-5-allyl-barbitursaeure (21248-32-8)

Guidance literature:

With sodium acetate;

Reference yield:

5,5-diallylbarbituric acid (52-43-7) → 5-Acetonyl-5-allyl-barbitursaeure (21248-32-8)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous H₂SO₄

2: K₂cr2O₇; aqueous H₂SO₄

With potassium dichromate; sulfuric acid;

upstream raw materials:

5-(2-oxopropyl)perhydropyrimidine-2,4,6-trione

allyl bromide

proxibarbal

5-allyl-5-(3-iodo-2-oxo-propyl)-barbituric acid