Me₃SnCH₂C(CH₂)PPh₂

Base Information

Chemical Name:Me₃SnCH₂C(CH₂)PPh₂
CAS No.:120726-27-4
Molecular Formula:C₁₈H₂₃PSn
Molecular Weight:389.064
Hs Code.:

Me<sub>3</sub>SnCH<sub>2</sub>C(CH<sub>2</sub>)PPh<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Me₃SnCH₂C(CH₂)PPh₂

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Technology Process of Me₃SnCH₂C(CH₂)PPh₂

There total 2 articles about Me₃SnCH₂C(CH₂)PPh₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 463-49-0
1,2-propanediene

: 1213-51-0
(trimethylstannyl)diphenylphosphine

: 129741-78-2
(E)-(trimethylstannyl-CH₂)(diphenylphosphino)CCHMe

: 120726-27-4
Me₃SnCH₂C(CH₂)PPh₂

Guidance literature:: byproducts: hexadimethyltin; Irradiation (UV/VIS); slow bubbling of gaseous allene through Sn-compd. under irradiation (TQ 150 high pressure mercury lamp) for 8 h at room temp.; monitored by (1)H NMR (total yield of regioisomers 78 %, ratio of diphenylphosphino/ diphenylphosphinomethyl isomer = 94/6);
DOI:10.1016/0022-328X(90)85241-P

Reference yield:

: 463-49-0
1,2-propanediene

: 1213-51-0
(trimethylstannyl)diphenylphosphine

: 120726-31-0
Ph₂PCH₂C(CH₂)SnMe₃

: 120726-27-4
Me₃SnCH₂C(CH₂)PPh₂

Guidance literature:: Irradiation (UV/VIS); characterised by NMR {(1)H, (13)C, (31)P, (119)Sn}, overall yield: 78%, ratio Me3SnCH2C(CH2)(PPh2)/(Ph2P)CH2C(CH2)SnMe3 = 89/11;
DOI:10.1016/0022-328X(88)80105-0