N,N'-Disalicylidene-1,3-phenylenediamine

Base Information

• Chemical Name: N,N'-Disalicylidene-1,3-phenylenediamine
• CAS No.: 17911-94-3
• Molecular Formula: C20H16N2O2
• Molecular Weight: 316.359
• DSSTox Substance ID: DTXSID901289921
• Nikkaji Number: J752.471D
• Mol file: 17911-94-3.mol

Synonyms:ChemDiv3_000211;SCHEMBL2492349;SCHEMBL2492350;DTXSID901289921;HMS1473J13;Bis(salicylidene)-m-phenylenediamine;STK749482;AKOS001590350;IDI1_019529;NCGC00177291-01;N,N'-Disalicylidene-1,3-phenylenediamine;BRD-K82954228-001-01-8;2,2'-{1,3-phenylenebis[nitrilo(E)methylylidene]}diphenol;2,2'-{benzene-1,3-diylbis[nitrilo(E)methylylidene]}diphenol;2-{(E)-[(3-{[(E)-(2-hydroxyphenyl)methylidene]amino}phenyl)imino]methyl}phenol;17911-94-3

Chemical Property of N,N'-Disalicylidene-1,3-phenylenediamine

Chemical Property:

• XLogP3: 4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 316.121177757
• Heavy Atom Count: 24
• Complexity: 399

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)C=NC2=CC(=CC=C2)N=CC3=CC=CC=C3O)O

Technology Process of N,N'-Disalicylidene-1,3-phenylenediamine

There total 3 articles about N,N'-Disalicylidene-1,3-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.9%

m-phenylenediamine (108-45-2,64554-26-3,76583-20-5) + salicylaldehyde (90-02-8) → 2,2'‐((1E,1'E)‐(1,3‐phenylenebis(azanylylidene))bis(methanylylidene))diphenol (17911-94-3)

Guidance literature:

With tin(II) chloride dihdyrate; In dichloromethane; at 20 ℃; for 6h;

DOI:10.1007/s12039-019-1645-2

Reference yield: 70.0%

m-phenylenediamine (108-45-2,64554-26-3,76583-20-5) + salicylaldehyde (90-02-8) → 1,3-Bis-salicylidenamino-benzol (17911-94-3)

Guidance literature:

for 2h; Heating;

Reference yield:

C40H30N4NiO2S2 → 1,3-Bis-salicylidenamino-benzol (17911-94-3) + C40H28N4Ni2S4

Guidance literature:

With oxygen; In water; at 25 ℃; for 480h; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.inorgchem.5b01334

upstream raw materials:

m-phenylenediamine

salicylaldehyde

Downstream raw materials:

{Co{(C₆H₄)(O)CHN(C₆H₄)NCH(C₆H₄)(OH)}Cl(H₂O)3}

{Cu{(C₆H₄)(O)CHN(C₆H₄)NCH(C₆H₄)(OH)}Cl(H₂O)}

{Ni{(C₆H₄)(O)CHN(C₆H₄)NCH(C₆H₄)(OH)}Cl(H₂O)3}

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