2,2-Diphenyl-1-oxa-2-silacyclohexane

Base Information

Chemical Name:2,2-Diphenyl-1-oxa-2-silacyclohexane
CAS No.:17933-86-7
Molecular Formula:C₁₆H₁₈OSi
Molecular Weight:254.404
Hs Code.:
DSSTox Substance ID:DTXSID601289110

Synonyms:2,2-Diphenyl-1-oxa-2-silacyclohexane;SCHEMBL35817;DTXSID601289110;17933-86-7

Suppliers and Price of 2,2-Diphenyl-1-oxa-2-silacyclohexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-Diphenyl-1-oxa-2-silacyclohexane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:254.112691728
Heavy Atom Count:18
Complexity:236

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC[Si](OC1)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of 2,2-Diphenyl-1-oxa-2-silacyclohexane

There total 8 articles about 2,2-Diphenyl-1-oxa-2-silacyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 144890-00-6
diphenyl(tetrahydrofuran-2-yl)silane

: 17933-86-7
1-oxa-2-sila-2,2-diphenylcyclohexane

Guidance literature:: With palladium/alumina; In hexane; for 15h; Ambient temperature;
DOI:10.1016/0022-328X(92)85060-A

Reference yield:

: 130648-87-2
<2-(4,5-dihydrofuryl)>diphenylsilane

: 17933-86-7
1-oxa-2-sila-2,2-diphenylcyclohexane

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / NaOH / 6 h / Heating

2: 71 percent / H₂ / 5percent Pd/Al₂O₃ / pentane / 10 h / 760 Torr / Ambient temperature

3: 37 percent / LiAlH₄ / diethyl ether / 4 h / Heating

4: 59 percent / 5percent Pd/Al₂O₃ / hexane / 15 h / Ambient temperature

With sodium hydroxide; palladium/alumina; lithium aluminium tetrahydride; hydrogen; palladium/alumina; In diethyl ether; hexane; pentane;
DOI:10.1016/0022-328X(92)85060-A

Reference yield:

: 144889-93-0
<2-(4,5-dihydrofuryl)>diphenylethoxysilane

: 17933-86-7
1-oxa-2-sila-2,2-diphenylcyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / H₂ / 5percent Pd/Al₂O₃ / pentane / 10 h / 760 Torr / Ambient temperature

2: 37 percent / LiAlH₄ / diethyl ether / 4 h / Heating

3: 59 percent / 5percent Pd/Al₂O₃ / hexane / 15 h / Ambient temperature

With palladium/alumina; lithium aluminium tetrahydride; hydrogen; palladium/alumina; In diethyl ether; hexane; pentane;
DOI:10.1016/0022-328X(92)85060-A