Benzoic acid, 3,4-bis(decyloxy)-, 4-carboxyphenyl ester

Base Information Edit

Chemical Name:Benzoic acid, 3,4-bis(decyloxy)-, 4-carboxyphenyl ester
CAS No.:180678-39-1
Molecular Formula:C34H50O6
Molecular Weight:554.767
Hs Code.:
Mol file:180678-39-1.mol

Synonyms:

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Chemical Property of Benzoic acid, 3,4-bis(decyloxy)-, 4-carboxyphenyl ester Edit

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Technology Process of Benzoic acid, 3,4-bis(decyloxy)-, 4-carboxyphenyl ester

There total 6 articles about Benzoic acid, 3,4-bis(decyloxy)-, 4-carboxyphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 180678-34-6
benzyl 4-(3,4-di-n-decyloxybenzoyloxy)benzoate

: 180678-39-1
4-(3,4-di-n-decyloxybenzoyloxy)benzoic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; for 3h;
DOI:10.1039/b503591k

Reference yield:

: 2150-43-8
3,4-dihydroxybenzoic acid methyl ester

: 180678-39-1
4-(3,4-di-n-decyloxybenzoyloxy)benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃; KI / dimethylformamide / 110 °C

2: aq. KOH / dioxane / 6 h / Heating

3: 4-(N,N-dimethylamino)pyridine; N,N'-dicyclohexylcarbodiimide / CH₂Cl₂ / 20 °C

4: cyclohexene; ethanol / Pd(OH)2/C / 8 h / Heating

With dmap; potassium hydroxide; ethanol; potassium carbonate; dicyclohexyl-carbodiimide; potassium iodide; cyclohexene; palladium dihydroxide; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; 1: Williamson etherification;
DOI:10.1021/ja0585477

Reference yield:

: 120878-42-4
3,4-di-n-decyloxybenzoic acid

: 180678-39-1
4-(3,4-di-n-decyloxybenzoyloxy)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 4-(N,N-dimethylamino)pyridine; N,N'-dicyclohexylcarbodiimide / CH₂Cl₂ / 20 °C

2: cyclohexene; ethanol / Pd(OH)2/C / 8 h / Heating

With dmap; ethanol; dicyclohexyl-carbodiimide; cyclohexene; palladium dihydroxide; In dichloromethane;
DOI:10.1021/ja0585477