Dimethyl 11-methyl-9,10-dihydro-9,10-ethanoanthracene-11,12-dicarboxylate

Base Information

Chemical Name:Dimethyl 11-methyl-9,10-dihydro-9,10-ethanoanthracene-11,12-dicarboxylate
CAS No.:5472-28-6
Molecular Formula:C₂₁H₂₀O₄
Molecular Weight:336.387
Hs Code.:
NSC Number:27933
DSSTox Substance ID:DTXSID00970037
ChEMBL ID:CHEMBL1904968

Synonyms:MLS002639195;5472-28-6;NSC27933;dimethyl 11-methyl-9,10-dihydro-9,10-ethanoanthracene-11,12-dicarboxylate;CHEMBL1904968;DTXSID00970037;HMS3080A03;NSC-27933;SMR001548642

Suppliers and Price of Dimethyl 11-methyl-9,10-dihydro-9,10-ethanoanthracene-11,12-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Dimethyl 11-methyl-9,10-dihydro-9,10-ethanoanthracene-11,12-dicarboxylate

Chemical Property:

Vapor Pressure:8.84E-10mmHg at 25°C
Boiling Point:449.7°Cat760mmHg
Flash Point:223.1°C
Density:1.217g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:336.13615911
Heavy Atom Count:25
Complexity:534

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C(C2C3=CC=CC=C3C1C4=CC=CC=C24)C(=O)OC)C(=O)OC

Technology Process of Dimethyl 11-methyl-9,10-dihydro-9,10-ethanoanthracene-11,12-dicarboxylate

There total 7 articles about Dimethyl 11-methyl-9,10-dihydro-9,10-ethanoanthracene-11,12-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120-12-7
anthracene

: 5472-28-6
(+/-)-11-methyl-9,10-dihydro-9,10-ethano-anthracene-dicarboxylic acid-(11r.12t)-dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: propionic acid / 145 °C

2: diethyl ether

With diethyl ether; propionic acid;
DOI:10.1021/ja01184a049

Reference yield:

: 498-24-8,7407-59-2
Mesaconic acid

: 5472-28-6
(+/-)-11-methyl-9,10-dihydro-9,10-ethano-anthracene-dicarboxylic acid-(11r.12t)-dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: propionic acid / 145 °C

2: diethyl ether

With diethyl ether; propionic acid;
DOI:10.1021/ja01184a049

Reference yield:

: 120-12-7
anthracene

: 5472-28-6
(+/-)-11-methyl-9,10-dihydro-9,10-ethano-anthracene-dicarboxylic acid-(11r.12c)-dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / Behandeln des Reaktionsprodukts mit wss. Kalilauge

2: diethyl ether

With diethyl ether; toluene;
DOI:10.1021/ja01184a049