Cyclopentanecarboxylic acid, 1-[[methoxy[[[(phenylmethoxy)carbonyl]amino]methyl]phosphinyl]methyl]- , 1,1-dimethylethyl ester

Base Information

Chemical Name:Cyclopentanecarboxylic acid, 1-[[methoxy[[[(phenylmethoxy)carbonyl]amino]methyl]phosphinyl]methyl]- , 1,1-dimethylethyl ester
CAS No.:182048-45-9
Molecular Formula:C₂₁H₃₂NO₆P
Molecular Weight:425.462
Hs Code.:
Mol file:182048-45-9.mol

Cyclopentanecarboxylic acid,
1-[[methoxy[[[(phenylmethoxy)carbonyl]amino]methyl]phosphinyl]methyl]-
, 1,1-dimethylethyl ester

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Chemical Property of Cyclopentanecarboxylic acid, 1-[[methoxy[[[(phenylmethoxy)carbonyl]amino]methyl]phosphinyl]methyl]- , 1,1-dimethylethyl ester

Chemical Property:

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Technology Process of Cyclopentanecarboxylic acid, 1-[[methoxy[[[(phenylmethoxy)carbonyl]amino]methyl]phosphinyl]methyl]- , 1,1-dimethylethyl ester

There total 3 articles about Cyclopentanecarboxylic acid, 1-[[methoxy[[[(phenylmethoxy)carbonyl]amino]methyl]phosphinyl]methyl]- , 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 107148-17-4
methyl N-benzyloxycarbonylaminomethylphosphinate

: 174767-44-3
t-Butyl 1-[(trifluoromethanesulfonyl)oxy]methylcyclopentanecarboxylate

: 182048-45-9
1-[(Benzyloxycarbonylamino-methyl)-methoxy-phosphinoylmethyl]-cyclopentanecarboxylic acid tert-butyl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran;
DOI:10.1016/0960-894X(96)00297-1

Reference yield:

: 131066-43-8
N-benzyloxycarbonylaminomethyl-H-phosphinic acid

: 182048-45-9
1-[(Benzyloxycarbonylamino-methyl)-methoxy-phosphinoylmethyl]-cyclopentanecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 10 percent / DEC, DMAP

2: 25 percent / NaH / tetrahydrofuran

With dmap; diethylcarbamazine; sodium hydride; In tetrahydrofuran;
DOI:10.1016/0960-894X(96)00297-1

Reference yield:

: 137613-90-2
t-Butyl 1-(Hydroxymethyl)cyclopentanecarboxylate

: 182048-45-9
1-[(Benzyloxycarbonylamino-methyl)-methoxy-phosphinoylmethyl]-cyclopentanecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridine; CH₂Cl₂ / -78 - 0 °C

2: 25 percent / NaH / tetrahydrofuran

With sodium hydride; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1016/0960-894X(96)00297-1