(+/-)-trans-3,4,4a,5,6,12c-hexahydro-2H-benzo[c]phenanthren-1-one-(2,4-dinitro-phenylhydrazone)

Base Information

Chemical Name:(+/-)-trans-3,4,4a,5,6,12c-hexahydro-2H-benzo[c]phenanthren-1-one-(2,4-dinitro-phenylhydrazone)
CAS No.:121968-91-0
Molecular Formula:C₂₄H₂₂N₄O₄
Molecular Weight:430.463
Hs Code.:

(+/-)-<i>trans</i>-3,4,4a,5,6,12<i>c</i>-hexahydro-2<i>H</i>-benzo[<i>c</i>]phenanthren-1-one-(2,4-dinitro-phenylhydrazone)

Synonyms:

Suppliers and Price of (+/-)-trans-3,4,4a,5,6,12c-hexahydro-2H-benzo[c]phenanthren-1-one-(2,4-dinitro-phenylhydrazone)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-trans-3,4,4a,5,6,12c-hexahydro-2H-benzo[c]phenanthren-1-one-(2,4-dinitro-phenylhydrazone)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-trans-3,4,4a,5,6,12c-hexahydro-2H-benzo[c]phenanthren-1-one-(2,4-dinitro-phenylhydrazone)

There total 3 articles about (+/-)-trans-3,4,4a,5,6,12c-hexahydro-2H-benzo[c]phenanthren-1-one-(2,4-dinitro-phenylhydrazone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40358-51-8
1-cyclohex-1-enyl-naphthalene

: 121968-91-0
(+/-)-trans-3,4,4a,5,6,12c-hexahydro-2H-benzo[c]phenanthren-1-one-(2,4-dinitro-phenylhydrazone)

Guidance literature:: Multi-step reaction with 4 steps

1: propionic acid; aqueous HCl / Erwaermen des Reaktionsprodukts mit aethanol. KOH und Erhitzen des danach erhaltenen Reaktionsprodukts mit wss. HCl, wss. Formaldehyd und Dioxan

2: xylene / Erhitzen des Reaktionsprodukts auf 200grad

3: HF

4: ether BF₃; dioxane / Erwaermen des Reaktionsprodukts mit Raney-Nickel in Aethanol und Behandeln des danach erhaltenen Ketons mit <2,4-Dinitro-phenyl>-hydrazin

With 1,4-dioxane; hydrogenchloride; boron trifluoride diethyl etherate; hydrogen fluoride; propionic acid; xylene;
DOI:10.1039/jr9570001293

Reference yield:

: 108842-56-4
2-(1-naphthyl)-2-cyclohexenone

: 121968-91-0
(+/-)-trans-3,4,4a,5,6,12c-hexahydro-2H-benzo[c]phenanthren-1-one-(2,4-dinitro-phenylhydrazone)

Guidance literature:: Multi-step reaction with 3 steps

1: xylene / Erhitzen des Reaktionsprodukts auf 200grad

2: HF

3: ether BF₃; dioxane / Erwaermen des Reaktionsprodukts mit Raney-Nickel in Aethanol und Behandeln des danach erhaltenen Ketons mit <2,4-Dinitro-phenyl>-hydrazin

With 1,4-dioxane; boron trifluoride diethyl etherate; hydrogen fluoride; xylene;
DOI:10.1039/jr9570001293

Reference yield:

: 109394-97-0
(+/-)-(2t-[1]naphthyl-3-oxo-cyclohex-r-yl)-acetic acid

: 121968-91-0
(+/-)-trans-3,4,4a,5,6,12c-hexahydro-2H-benzo[c]phenanthren-1-one-(2,4-dinitro-phenylhydrazone)

Guidance literature:: Multi-step reaction with 2 steps

1: HF

2: ether BF₃; dioxane / Erwaermen des Reaktionsprodukts mit Raney-Nickel in Aethanol und Behandeln des danach erhaltenen Ketons mit <2,4-Dinitro-phenyl>-hydrazin

With 1,4-dioxane; boron trifluoride diethyl etherate; hydrogen fluoride;
DOI:10.1039/jr9570001293