carbonylhydridobis(triphenyl phosphite)(triphenyl phosphito-(C⁽²⁾P))ruthenium(II)

Base Information

• Chemical Name: carbonylhydridobis(triphenyl phosphite)(triphenyl phosphito-(C⁽²⁾P))ruthenium(II)
• CAS No.: 59634-27-4
• Molecular Formula: C₅₅H₄₅O₁₀P₃Ru
• Molecular Weight: 1059.95

Synonyms:

Chemical Property of carbonylhydridobis(triphenyl phosphite)(triphenyl phosphito-(C⁽²⁾P))ruthenium(II)

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of carbonylhydridobis(triphenyl phosphite)(triphenyl phosphito-(C⁽²⁾P))ruthenium(II)

There total 2 articles about carbonylhydridobis(triphenyl phosphite)(triphenyl phosphito-(C⁽²⁾P))ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triphenyl phosphite (101-02-0) + carbonyldihydridotris(triphenylphosphine)ruthenium(II) (22337-78-6) → carbonylhydrido(triphenylphosphine)(triphenyl phosphite)(triphenylphosphito-(C(2)P))ruthenium(II) + carbonylhydridobis(triphenyl phosphite)(triphenyl phosphito-(C(2)P))ruthenium(II) (59634-27-4)

Guidance literature:

In xylene; N2-atmosphere; refluxing for 1 h; evapn. (reduced pressure, room temp.), washing (hexane), recrystn. (CH2Cl2/MeOH); product mixt. not sepd., detd. by (1)H- and (31)P-NMR spectroscopy; total yield 40 %; elem. anal.;

DOI:10.1039/DT9760000613

Reference yield:

triphenyl phosphite (101-02-0) + tricarbonylbis(triphenylphosphine)ruthenium(0) (20332-49-4,14741-36-7) → carbonylhydrido(triphenylphosphine)(triphenyl phosphite)(triphenylphosphito-(C(2)P))ruthenium(II) + carbonylhydridobis(triphenyl phosphite)(triphenyl phosphito-(C(2)P))ruthenium(II) (59634-27-4)

Guidance literature:

In xylene; N2-atmosphere; refluxing for 1 h; evapn. (reduced pressure, room temp.), washing (hexane), recrystn. (CH2Cl2/MeOH); product mixt. not sepd., detd. by (1)H- and (31)P-NMR spectroscopy; total yield 28 %;

DOI:10.1039/DT9760000613

upstream raw materials:

triphenyl phosphite

carbonyldihydridotris(triphenylphosphine)ruthenium(II)

tricarbonylbis(triphenylphosphine)ruthenium⁽⁰⁾

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