azido[2-(diphenylphosphino)benzaldehyde semicarbazonato-κ3P,N1,O]nickel(II)

Base Information

• Chemical Name: azido[2-(diphenylphosphino)benzaldehyde semicarbazonato-κ3P,N1,O]nickel(II)
• CAS No.: 1188591-58-3
• Molecular Formula: C₂₀H₁₇N₆NiOP
• Molecular Weight: 447.058

Synonyms:

Chemical Property of azido[2-(diphenylphosphino)benzaldehyde semicarbazonato-κ3P,N1,O]nickel(II)

Chemical Property:

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Technology Process of azido[2-(diphenylphosphino)benzaldehyde semicarbazonato-κ3P,N1,O]nickel(II)

There total 1 articles about azido[2-(diphenylphosphino)benzaldehyde semicarbazonato-κ3P,N1,O]nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium azide + nickel(II) nitrate hexahydrate + 2-(diphenylphosphino)benzaldehyde semicarbazone → azido[2-(diphenylphosphino)benzaldehyde semicarbazonato-κ3P,N1,O]nickel(II) (1188591-58-3)

Guidance literature:

In ethanol; Ni(NO3)2*6H2O and appropriate semicarbazone dissolved in MeOH under heating, warm soln. of NaN3 in MeOH added; white ppt. transformed into red crystals after 24 h, crystals filtered off, washed with MeOH;

DOI:10.1107/S0108270109021970

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