[(p-octa-tert-butylphenyl corrolazine)Mn(III)]*CH₃OH

Base Information

• Chemical Name: [(p-octa-tert-butylphenyl corrolazine)Mn(III)]*CH₃OH
• CAS No.: 858342-92-4
• Molecular Formula: C₉₇H₁₀₈MnN₇O
• Molecular Weight: 1442.91
• Mol file: 858342-92-4.mol

Synonyms:

Chemical Property of [(p-octa-tert-butylphenyl corrolazine)Mn(III)]*CH₃OH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(p-octa-tert-butylphenyl corrolazine)Mn(III)]*CH₃OH

There total 1 articles about [(p-octa-tert-butylphenyl corrolazine)Mn(III)]*CH₃OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

octakis(para-tert-butylphenyl)corrolazine (370569-23-6) + manganese(III) acetylacetonate (14284-89-0) → [(p-octa-tert-butylphenyl corrolazine)Mn(III)]*CH3OH (858342-92-4)

Guidance literature:

In methanol; dichloromethane; Mn complex was added to soln. ligand in CH2Cl2/MeOH (90:10), mixt. was stirried at room temp. for 18 h; solvent was evapd., product was chromd. on SiO2 (CH2Cl2/MeOH, 99:1); elem. anal.;

DOI:10.1021/ic0503636

Reference yield:

[(p-octa-tert-butylphenyl corrolazine)Mn(III)]*CH3OH (858342-92-4) + toluene (108-88-3,15644-74-3,16713-13-6) → [(p-octa-tert-butylphenyl corrolazine0Mn(III)]*CH3OH*(C7H8)3

Guidance literature:

In methanol; toluene;

DOI:10.1021/ic0503636

upstream raw materials:

octakis(para-tert-butylphenyl)corrolazine

manganese(III) acetylacetonate