3-Azido-1,5,5-trimethyl-1-cyclohexene

Base Information

Chemical Name:3-Azido-1,5,5-trimethyl-1-cyclohexene
CAS No.:185447-96-5
Molecular Formula:C9H15N3
Molecular Weight:165.238
Hs Code.:
DSSTox Substance ID:DTXSID30447166
Nikkaji Number:J789.361B

Synonyms:3-Azido-1,5,5-trimethyl-1-cyclohexene;185447-96-5;DTXSID30447166;JEJFZVQTFXLFMN-UHFFFAOYSA-N;3,5,5-Trimethyl-2-cyclohexenyl azide

Suppliers and Price of 3-Azido-1,5,5-trimethyl-1-cyclohexene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Azido-1,5,5-trimethyl-1-cyclohexene

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:165.126597491
Heavy Atom Count:12
Complexity:247

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(CC(C1)(C)C)N=[N+]=[N-]

Technology Process of 3-Azido-1,5,5-trimethyl-1-cyclohexene

There total 5 articles about 3-Azido-1,5,5-trimethyl-1-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 19687-18-4
acetic acid 3,5,5-trimethylcyclohex-2-enyl ester

: 4648-54-8
trimethylsilylazide

: 185447-96-5
1-azido-3,5,5-trimethylcyclohex-2-ene

Guidance literature:: With magnesium bis(trifluoromethane solfonyl)imide; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1016/S0040-4039(97)00441-3

Reference yield: 89.0%

: 470-99-5
isophorol

: 185447-96-5
1-azido-3,5,5-trimethylcyclohex-2-ene

Guidance literature:: With MoCl₂(acetylacetonate)2; trimethylsilylazide; silver trifluoromethanesulfonate; In dichloromethane; for 0.166667h; Ambient temperature;
DOI:10.1021/jo990372u

Reference yield: 71.0%

: 19687-18-4
acetic acid 3,5,5-trimethylcyclohex-2-enyl ester

: 185447-96-5
1-azido-3,5,5-trimethylcyclohex-2-ene

Guidance literature:: With trimethylsilylazide; LiCo(B₉C₂H₁₁)2; In 1,2-dichloro-ethane; for 0.5h; Ambient temperature;
DOI:10.1016/S0040-4039(96)02021-7