Methanediamine, 1-(4-bromophenyl)-N,N'-bis[(4-bromophenyl)methylene]-

Base Information

• Chemical Name: Methanediamine, 1-(4-bromophenyl)-N,N'-bis[(4-bromophenyl)methylene]-
• CAS No.: 185459-60-3
• Molecular Formula: C21H15Br3N2
• Molecular Weight: 535.076
• Mol file: 185459-60-3.mol

Synonyms:

Chemical Property of Methanediamine, 1-(4-bromophenyl)-N,N'-bis[(4-bromophenyl)methylene]-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methanediamine, 1-(4-bromophenyl)-N,N'-bis[(4-bromophenyl)methylene]-

There total 1 articles about Methanediamine, 1-(4-bromophenyl)-N,N'-bis[(4-bromophenyl)methylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-bromo-benzaldehyde (1122-91-4) → N,N'-bis(4-bromobenzylidene)-1-(4-bromophenyl)methanediamine (185459-60-3)

Guidance literature:

With ammonium hydroxide; at 25 ℃; for 48h;

DOI:10.1002/ejoc.201901325

Reference yield: 97.0%

N,N'-bis(4-bromobenzylidene)-1-(4-bromophenyl)methanediamine (185459-60-3) → 4,4'-dibromodibenzylamine (24898-17-7)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; for 2h;

DOI:10.1016/j.tetlet.2008.09.048

Reference yield: 94.0%

N,N'-bis(4-bromobenzylidene)-1-(4-bromophenyl)methanediamine (185459-60-3) → 2,4,5-tris(4-bromophenyl)imidazole (36741-16-9)

Guidance literature:

With potassium tert-butylate; oxygen; In dimethyl sulfoxide; for 12h; Heating;

DOI:10.1023/A:1023915024572

upstream raw materials:

4-bromo-benzaldehyde

Downstream raw materials:

2,5-di(4-bromophenyl)-3,3,4,4-tetracyanopyrrolidine

2,4,5-tris(4-bromophenyl)imidazole

4,4'-dibromodibenzylamine

1,3-bis(4-bromophenyl)-2,3-dihydro-1H-naphtho[1,2-e][1,3]oxazine