phenylsulfanyl-acetaldehyde-(2,4-dinitro-phenylhydrazone)

Base Information

• Chemical Name: phenylsulfanyl-acetaldehyde-(2,4-dinitro-phenylhydrazone)
• CAS No.: 66303-53-5
• Molecular Formula: C₁₄H₁₂N₄O₄S
• Molecular Weight: 332.34
• Mol file: 66303-53-5.mol

Synonyms:

Chemical Property of phenylsulfanyl-acetaldehyde-(2,4-dinitro-phenylhydrazone)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenylsulfanyl-acetaldehyde-(2,4-dinitro-phenylhydrazone)

There total 2 articles about phenylsulfanyl-acetaldehyde-(2,4-dinitro-phenylhydrazone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thiophenol (108-98-5) → phenylsulfanyl-acetaldehyde-(2,4-dinitro-phenylhydrazone) (66303-53-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium iodide; sodium ethylate; ethanol

2: aq.-ethanolic H₂SO₄

With ethanol; sulfuric acid; sodium ethanolate; sodium iodide;

Reference yield:

phenylmercaptoacetaldehyde dimethyl acetal (99172-76-6) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → phenylsulfanyl-acetaldehyde-(2,4-dinitro-phenylhydrazone) (66303-53-5)

Guidance literature:

With sulfuric acid;

upstream raw materials:

phenylmercaptoacetaldehyde dimethyl acetal

(2,4-dinitro-phenyl)-hydrazine

thiophenol