(+/-)-N,N'-bis-(trans-4-phenyl-[1,3]dioxan-5-yl)-urea

Base Information

Chemical Name:(+/-)-N,N'-bis-(trans-4-phenyl-[1,3]dioxan-5-yl)-urea
CAS No.:115019-79-9
Molecular Formula:C₂₁H₂₄N₂O₅
Molecular Weight:384.432
Hs Code.:

(+/-)-<i>N</i>,<i>N</i>'-bis-(<i>trans</i>-4-phenyl-[1,3]dioxan-5-yl)-urea

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-N,N'-bis-(trans-4-phenyl-[1,3]dioxan-5-yl)-urea

Chemical Property:

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Technology Process of (+/-)-N,N'-bis-(trans-4-phenyl-[1,3]dioxan-5-yl)-urea

There total 3 articles about (+/-)-N,N'-bis-(trans-4-phenyl-[1,3]dioxan-5-yl)-urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2231-67-6,92057-56-2
(+/-)-trans-4-phenyl-[1,3]dioxane-5-carboxylic acid

: 115019-79-9
(+/-)-N,N'-bis-(trans-4-phenyl-[1,3]dioxan-5-yl)-urea

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: water containing hydrazine hydrate / 110 °C

3: acetic acid; aqueous sodium nitrite solution / Erwaermen des Reaktionsprodukts mit wss. Natronlauge

With diethyl ether; hydrazine hydrate; acetic acid; sodium nitrite;

Reference yield:

: 140-10-3
(E)-3-phenylacrylic acid

: 115019-79-9
(+/-)-N,N'-bis-(trans-4-phenyl-[1,3]dioxan-5-yl)-urea

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; concentrated sulfuric acid

2: diethyl ether

3: water containing hydrazine hydrate / 110 °C

4: acetic acid; aqueous sodium nitrite solution / Erwaermen des Reaktionsprodukts mit wss. Natronlauge

With diethyl ether; sulfuric acid; hydrazine hydrate; acetic acid; sodium nitrite;

Reference yield:

: 104665-62-5
(+/-)-trans-4-phenyl-[1,3]dioxane-5-carboxylic acid methyl ester

: 115019-79-9
(+/-)-N,N'-bis-(trans-4-phenyl-[1,3]dioxan-5-yl)-urea

Guidance literature:: Multi-step reaction with 2 steps

1: water containing hydrazine hydrate / 110 °C

2: acetic acid; aqueous sodium nitrite solution / Erwaermen des Reaktionsprodukts mit wss. Natronlauge

With hydrazine hydrate; acetic acid; sodium nitrite;