Technology Process of 2,4-Pentadienoic acid, 2-(acetylamino)-5-phenyl-, methyl ester, (Z,E)-
There total 9 articles about 2,4-Pentadienoic acid, 2-(acetylamino)-5-phenyl-, methyl ester, (Z,E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
styrene; Methyl 2-acetamidoacrylate;
With
silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate;
In
tert-Amyl alcohol;
at 120 ℃;
for 16h;
Inert atmosphere;
closed reactor;
With
ammonium acetate;
In
tert-Amyl alcohol;
at 20 ℃;
for 1h;
diastereoselective reaction;
Inert atmosphere;
DOI:10.1002/chem.201101340
- Guidance literature:
-
methyl 2-acetylamino-2-(dimethoxyphosphinyl)acetate;
With
1,1,3,3-tetramethylguanidine;
In
tetrahydrofuran;
at -78 ℃;
for 0.25h;
(E)-3-phenylpropenal;
In
tetrahydrofuran;
at -78 - 25 ℃;
for 4h;
- Guidance literature:
-
Methyl 2-(N-Benzoylamino)-2-(dimethoxyphosphinyl)ethanoate;
With
N,N,N',N'-tetramethylguanidine;
In
tetrahydrofuran;
at -78 ℃;
for 0.25h;
(E)-3-phenylpropenal;
In
tetrahydrofuran;
at -78 - 25 ℃;
for 4h;
