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Technology Process of C6H4NHCOC6H4CH2(N(CH)2CHN)FeC20H2N4(CH3)4(C2H5)4C6H4NHCOC6H3(C(OH)NC4H9)2

C6H4NHCOC6H4CH2(N(CH)2CHN)FeC20H2N4(CH3)4(C2H5)4C6H4NHCOC6H3(C(OH)NC4H9)2

Base Information
  • Chemical Name:C6H4NHCOC6H4CH2(N(CH)2CHN)FeC20H2N4(CH3)4(C2H5)4C6H4NHCOC6H3(C(OH)NC4H9)2
  • CAS No.:92139-08-7
  • Molecular Formula:C72H76FeN10O4
  • Molecular Weight:1201.31
  • Hs Code.:
C<sub>6</sub>H<sub>4</sub>NHCOC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>(N(CH)2CHN)FeC<sub>20</sub>H<sub>2</sub>N<sub>4</sub>(CH<sub>3</sub>)4(C<sub>2</sub>H<sub>5</sub>)4C<sub>6</sub>H<sub>4</sub>NHCOC<sub>6</sub>H<sub>3</sub>(C(OH)NC<sub>4</sub>H<sub>9</sub>)2

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Chemical Property of C6H4NHCOC6H4CH2(N(CH)2CHN)FeC20H2N4(CH3)4(C2H5)4C6H4NHCOC6H3(C(OH)NC4H9)2
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Technology Process of C6H4NHCOC6H4CH2(N(CH)2CHN)FeC20H2N4(CH3)4(C2H5)4C6H4NHCOC6H3(C(OH)NC4H9)2

There total 1 articles about C6H4NHCOC6H4CH2(N(CH)2CHN)FeC20H2N4(CH3)4(C2H5)4C6H4NHCOC6H3(C(OH)NC4H9)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans-5-(o-aminophenyl)-15-(o-<m-(N-imidazolylmethyl)benzamido>phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphinato-iron(II)

trans-5-(o-aminophenyl)-15-(o-phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphinato-iron(II)

trimesic acid di(n-butylamide)
92180-30-8

trimesic acid di(n-butylamide)

C<sub>6</sub>H<sub>4</sub>NHCOC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>(N(CH)2CHN)FeC<sub>20</sub>H<sub>2</sub>N<sub>4</sub>(CH<sub>3</sub>)4(C<sub>2</sub>H<sub>5</sub>)4C<sub>6</sub>H<sub>4</sub>NHCOC<sub>6</sub>H<sub>3</sub>(C(OH)NC<sub>4</sub>H<sub>9</sub>)2
92139-08-7

C6H4NHCOC6H4CH2(N(CH)2CHN)FeC20H2N4(CH3)4(C2H5)4C6H4NHCOC6H3(C(OH)NC4H9)2

Guidance literature:
With sodium dithionite; chloroformic acid ethyl ester; triethylamine; after reaction at 0°C (2 h) and at room temp. for further 3 d, the intermediately formed Fe(III)-compound was reduced by addn. of 6 moles Na2S2O4 per mole Fe(III) at pH 10 (buffer: 0.2 M Na2CO3/NaHCO3/ethylene glycole (1:1) or DMF/H2O (9:1));;
DOI:10.1246/cl.1984.997
upstream raw materials:

trimesic acid di(n-butylamide)

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