4,5-Bis(dodecyloxy)benzene-1,2-diamine

Base Information

Chemical Name:4,5-Bis(dodecyloxy)benzene-1,2-diamine
CAS No.:190435-62-2
Molecular Formula:C30H56N2O2
Molecular Weight:476.787
Hs Code.:
DSSTox Substance ID:DTXSID60571605
Nikkaji Number:J832.876E
Wikidata:Q82459749
Mol file:190435-62-2.mol

Synonyms:190435-62-2;1,2-Benzenediamine, 4,5-bis(dodecyloxy)-;4,5-BIS(DODECYLOXY)BENZENE-1,2-DIAMINE;4,5-didodecoxybenzene-1,2-diamine;1,2-Bis(dodecyloxy)-4,5-diaminobenzene;SCHEMBL2252027;DTXSID60571605;WVIOQJYIZWNFIG-UHFFFAOYSA-N;AMY27137;4,5-Bis-dodecyloxy benzene-1,2-diamine

Suppliers and Price of 4,5-Bis(dodecyloxy)benzene-1,2-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4,5-Bis(dodecyloxy)benzene-1,2-diamine

Chemical Property:

XLogP3:11.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:24
Exact Mass:476.43417903
Heavy Atom Count:34
Complexity:383

Purity/Quality:: 99.3% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCCCCCOC1=C(C=C(C(=C1)N)N)OCCCCCCCCCCCC

Technology Process of 4,5-Bis(dodecyloxy)benzene-1,2-diamine

There total 4 articles about 4,5-Bis(dodecyloxy)benzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 171418-24-9
1,2-bis(dodecyloxy)-4,5-dinitrobenzene

: 190435-62-2
4,5-bis(dodecyloxy)benzene-1,2-diamine

Guidance literature:: With palladium 10% on activated carbon; hydrazine hydrate; In ethanol; at 70 ℃; Inert atmosphere;
DOI:10.1071/CH13147

Reference yield:

: 42244-53-1
1,2-bisdodecyloxybenzene

: 190435-62-2
4,5-bis(dodecyloxy)benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / nitric acid; acetic acid / CH₂Cl₂; H₂O / 0 - 20 °C

2: 90 percent / hydrogen / Pd/C / ethanol / 24 h / 1520 Torr / Heating

With hydrogen; nitric acid; acetic acid; palladium on activated charcoal; In ethanol; dichloromethane; water;
DOI:10.1021/jo035840l

Reference yield:

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 190435-62-2
4,5-bis(dodecyloxy)benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / potassium carbonate / acetone / 48 h / Heating

2: 72 percent / nitric acid; acetic acid / CH₂Cl₂; H₂O / 0 - 20 °C

3: 90 percent / hydrogen / Pd/C / ethanol / 24 h / 1520 Torr / Heating

With hydrogen; nitric acid; potassium carbonate; acetic acid; palladium on activated charcoal; In ethanol; dichloromethane; water; acetone;
DOI:10.1021/jo035840l