[ReBHr₂(SiEt₃)(NO)(2,2'-bis(diphenylphosphino)diphenyl ether)]

Base Information

• Chemical Name: [ReBHr₂(SiEt₃)(NO)(2,2'-bis(diphenylphosphino)diphenyl ether)]
• CAS No.: 1308304-88-2
• Molecular Formula: C₄₂H₄₅BrNO₂P₂ReSi
• Molecular Weight: 951.969
• Mol file: 1308304-88-2.mol

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Chemical Property of [ReBHr₂(SiEt₃)(NO)(2,2'-bis(diphenylphosphino)diphenyl ether)]

Chemical Property:

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Technology Process of [ReBHr₂(SiEt₃)(NO)(2,2'-bis(diphenylphosphino)diphenyl ether)]

There total 1 articles about [ReBHr₂(SiEt₃)(NO)(2,2'-bis(diphenylphosphino)diphenyl ether)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethylsilane (617-86-7) + [ReBr2(MeCN)(NO)(2,2'-bis(diphenylphosphino)diphenyl ether)] → [ReBHr2(SiEt3)(NO)(2,2'-bis(diphenylphosphino)diphenyl ether)] (1308304-88-2)

Guidance literature:

In tetrahydrofuran-d8; byproducts: MeCN, BrSiEt3; Sonication; (N2); std. Schlenk technique; suspn. of Re complex and Si compd. in THF-d8 in NMR tube was sonicated at 50°C for 1 h; NMR monitoring; not isolated;

DOI:10.1021/om200092y

upstream raw materials:

triethylsilane