ledol

Base Information

• Chemical Name: ledol
• CAS No.: 19078-39-8
• Molecular Formula: C₁₅H₂₆O
• Molecular Weight: 222.371
• Mol file: 19078-39-8.mol

Synonyms:

Chemical Property of ledol

Chemical Property:

• Boiling Point: 293.9±8.0 °C(Predicted)
• PKA: 15.21±0.60(Predicted)
• PSA: 0.00000
• Density: 0.962±0.06 g/cm3(Predicted)
• LogP: 0.00000

Purity/Quality:

99% ^*data from raw suppliers

Ledol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ledol

There total 3 articles about ledol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

alloaromadendrene (25246-27-9) → ledol (489-41-8,552-02-3,577-27-5,19078-39-8,51371-47-2,55659-76-2,64366-31-0,64665-36-7,77171-54-1,88728-58-9,133443-04-6,146864-34-8) + (+)-viridiflorol (489-41-8,552-02-3,577-27-5,19078-39-8,51371-47-2,55659-76-2,64366-31-0,64665-36-7,77171-54-1,88728-58-9,133443-04-6,146864-34-8)

Guidance literature:

With lithium aluminium tetrahydride; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction. Yields of byproduct given; 1.) CHCl₃, RT, 30 min, 2.) Et₂O, RT, overnight;

DOI:10.1016/0040-4020(95)01079-3

Reference yield:

alloaromadendrene (25246-27-9) → ledol (489-41-8,552-02-3,577-27-5,19078-39-8,51371-47-2,55659-76-2,64366-31-0,64665-36-7,77171-54-1,88728-58-9,133443-04-6,146864-34-8) + (+)-viridiflorol (489-41-8,552-02-3,577-27-5,19078-39-8,51371-47-2,55659-76-2,64366-31-0,64665-36-7,77171-54-1,88728-58-9,133443-04-6,146864-34-8)

Guidance literature:

With lithium aluminium tetrahydride; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction. Yields of byproduct given; 1.) CHCl₃, RT, 30 min, 2.) Et₂O, RT, overnight;

DOI:10.1016/0040-4020(95)01079-3

Reference yield:

alloaromadendrene (25246-27-9) → ledol (489-41-8,552-02-3,577-27-5,19078-39-8,51371-47-2,55659-76-2,64366-31-0,64665-36-7,77171-54-1,88728-58-9,133443-04-6,146864-34-8)

Guidance literature:

Multistep reaction; (i) PhCO₃H, CHCl₃, (ii) LiAlH₄, Et₂O;

upstream raw materials:

alloaromadendrene

Downstream raw materials:

ledene

(1aR)-4c-phenylcarbamoyloxy-1.1.4t.7c-tetramethyl-(1arH.4atH.7atH.7bcH)-decahydro-1H-cycloprop[e]-azulene

Refernces