Zn(C₄NCC₆H₁₃CH₃)4H₂(C₆H₃(OCH₃)2)2

Base Information

• Chemical Name: Zn(C₄NCC₆H₁₃CH₃)4H₂(C₆H₃(OCH₃)2)2
• CAS No.: 1350823-36-7
• Molecular Formula: C₆₄H₈₄N₄O₄Zn
• Molecular Weight: 1038.79

Synonyms:

Chemical Property of Zn(C₄NCC₆H₁₃CH₃)4H₂(C₆H₃(OCH₃)2)2

Chemical Property:

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Technology Process of Zn(C₄NCC₆H₁₃CH₃)4H₂(C₆H₃(OCH₃)2)2

There total 1 articles about Zn(C₄NCC₆H₁₃CH₃)4H₂(C₆H₃(OCH₃)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(C4NCC6H13CH3)4H4(C6H3(OCH3)2)2 + zinc(II) acetate dihydrate (5970-45-6) → Zn(C4NCC6H13CH3)4H2(C6H3(OCH3)2)2 (1350823-36-7)

Guidance literature:

In methanol; chloroform; excess of Zn-contg. compd. (ca. 5 equivs.) was added to a stirred soln. of a ligand (1 equiv.) in CHCl3-MeOH soln. (10% MeOH); the mixt. was refluxed for 20 min; the soln. was washed with H2O, dried over Na2SO4, filtered and passed through a plug of silica gel; the solvent was removed under reduced pressure; column chromy. over silica gel; recrystn.;

DOI:10.1039/c1dt10880h

upstream raw materials:

zinc(II) acetate dihydrate

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