2-Propenoic acid, 3-phenyl-, 2-(1-oxo-3-phenyl-2-propenyl)hydrazide

Base Information

• Chemical Name: 2-Propenoic acid, 3-phenyl-, 2-(1-oxo-3-phenyl-2-propenyl)hydrazide
• CAS No.: 19473-98-4
• Molecular Formula: C₁₈H₁₆N₂O₂
• Molecular Weight: 292.337
• Hs Code.: 2929900090
• Mol file: 19473-98-4.mol

Synonyms:(E)-3-Phenyl-acrylic acid N'-[(E)-(3-phenyl-acryloyl)]-hydrazide;

Chemical Property of 2-Propenoic acid, 3-phenyl-, 2-(1-oxo-3-phenyl-2-propenyl)hydrazide

Chemical Property:

• PSA: 58.20000
• LogP: 3.34240

Purity/Quality:

(2Z)-3-Phenyl-N'-[(2E)-3-phenylprop-2-enoyl]prop-2-enehydrazide tech ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Propenoic acid, 3-phenyl-, 2-(1-oxo-3-phenyl-2-propenyl)hydrazide

There total 2 articles about 2-Propenoic acid, 3-phenyl-, 2-(1-oxo-3-phenyl-2-propenyl)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Cinnamoyl chloride (102-92-1,17082-09-6) → N,N'-di-trans-cinnamoyl-hydrazine (19473-98-4)

Guidance literature:

With tetrahydrofuran; sodium hydroxide; sulfuric acid; hydrazine;

DOI:10.1002/hlca.19690520625

Reference yield:

→ N,N'-Dicinnamoylhydrazin (19473-98-4)

Guidance literature:

Hydrazinsulfat, wss. NaOH, Zimtsaeurechlorid, THF (neben geringer Menge einer Verb. m. F: 285grad (Zers., unkorr.));

DOI:10.1002/hlca.19690520625

Reference yield: 70.0%

N,N'-di-trans-cinnamoyl-hydrazine (19473-98-4) → 2,5-bis[(E)-2-phenylethenyl]-1,3,5-oxadiazole (19473-91-7)

Guidance literature:

With trichlorophosphate; for 2h; Heating;

DOI:10.1134/S1070428007070172

upstream raw materials:

Cinnamoyl chloride

Downstream raw materials:

2,5-bis[(E)-2-phenylethenyl]-1,3,5-oxadiazole