Benzene, 1-bromo-3-(chloromethyl)-2,5-dimethoxy-

Base Information

Chemical Name:Benzene, 1-bromo-3-(chloromethyl)-2,5-dimethoxy-
CAS No.:196302-52-0
Molecular Formula:C9H10BrClO2
Molecular Weight:265.534
Hs Code.:
Mol file:196302-52-0.mol

Synonyms:3-Bromo-2,5-dimethoxybenzyl Chloride;1-bromo-3-chloromethyl-2,5-dimethoxy-benzene;

Suppliers and Price of Benzene, 1-bromo-3-(chloromethyl)-2,5-dimethoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1-bromo-3-(chloromethyl)-2,5-dimethoxy-

Chemical Property:

Boiling Point:317.1±37.0 °C(Predicted)
PSA：18.46000
Density:1.464±0.06 g/cm3(Predicted)
LogP:3.20510

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzene, 1-bromo-3-(chloromethyl)-2,5-dimethoxy-

There total 2 articles about Benzene, 1-bromo-3-(chloromethyl)-2,5-dimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 196302-51-9
(3-Bromo-2,5-dimethoxy-phenyl)-methanol

: 196302-52-0
1-Bromo-3-chloromethyl-2,5-dimethoxy-benzene

Guidance literature:: With thionyl chloride; zinc(II) chloride; In tetrahydrofuran; ethyl acetate;

Reference yield:

: 196302-52-0
1-Bromo-3-chloromethyl-2,5-dimethoxy-benzene

Guidance literature:

Reference yield:

: 196302-52-0
1-Bromo-3-chloromethyl-2,5-dimethoxy-benzene

: 551001-76-4
5-hydroxy-2-(4-hydroxy-phenyl)-7-methoxy-benzofuran-4-carbaldehyde oxime

Guidance literature:: Multi-step reaction with 8 steps

1: dimethylformamide

2: aq. H₂SO₄; AcOH

3: SOCl₂ / CH₂Cl₂

4: AlCl₃

5: pyridine hydrobromide / Heating

6: CuBr

7: POCl₃

8: NH₂OH

With aluminium trichloride; thionyl chloride; sulfuric acid; hydroxylamine; Pyridine hydrobromide; acetic acid; copper(I) bromide; trichlorophosphate; In dichloromethane; N,N-dimethyl-formamide; 4: Friedel-Crafts reaction;
DOI:10.1016/j.bmcl.2004.07.029