MoO(ClC₆H₄C(O)NHNCHC₆H₄O)Cl₂

Base Information

• Chemical Name: MoO(ClC₆H₄C(O)NHNCHC₆H₄O)Cl₂
• CAS No.: 98628-71-8
• Molecular Formula: C₁₄H₁₀Cl₃MoN₂O₃
• Molecular Weight: 456.544
• Mol file: 98628-71-8.mol

Synonyms:

Chemical Property of MoO(ClC₆H₄C(O)NHNCHC₆H₄O)Cl₂

Chemical Property:

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Useful:

Technology Process of MoO(ClC₆H₄C(O)NHNCHC₆H₄O)Cl₂

There total 1 articles about MoO(ClC₆H₄C(O)NHNCHC₆H₄O)Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ammonium oxopentachloromolybdate + 4-chloro-N’-(2-hydroxybenzylidene)benzohydrazide (100622-79-5) → MoO(ClC6H4C(O)NHNCHC6H4O)Cl2 (98628-71-8)

Guidance literature:

In ethanol; dissoln. of Schiff base by refluxing in ethanol; passing N2 through soln.; addn. of ammonium oxopentachloromolybdate; refluxing in N2, 1h; coolin; keeping in a vac. desiccator over solid KOH, 2-3 d; crystn.; filtration; washing (small amt. of dry ethanol); drying in vac. over solid KOH; elem. anal.;

upstream raw materials:

4-chloro-N’-(2-hydroxybenzylidene)benzohydrazide

Refernces