tetrakis(μ-3,5-dinitrobenzoato-κ2O:O')bis[(3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione-κO2)copper(II)]

Base Information

• Chemical Name: tetrakis(μ-3,5-dinitrobenzoato-κ2O:O')bis[(3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione-κO2)copper(II)]
• CAS No.: 934282-29-8
• Molecular Formula: C₄₄H₃₂Cu₂N₁₆O₂₈
• Molecular Weight: 1359.92
• Mol file: 934282-29-8.mol

Synonyms:

Chemical Property of tetrakis(μ-3,5-dinitrobenzoato-κ2O:O')bis[(3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione-κO2)copper(II)]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetrakis(μ-3,5-dinitrobenzoato-κ2O:O')bis[(3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione-κO2)copper(II)]

There total 1 articles about tetrakis(μ-3,5-dinitrobenzoato-κ2O:O')bis[(3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione-κO2)copper(II)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[Cu2(OAc)4(H2O)2] (879089-16-4,155065-88-6) + 3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione (58-08-2,138455-22-8,95789-13-2) + 3,5-dinitrobenzoic acid (99-34-3) → tetrakis(μ-3,5-dinitrobenzoato-κ2O:O')bis[(3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione-κO2)copper(II)] (934282-29-8)

Guidance literature:

In water; caffeine (0.5 mmol) added to aq. soln. of copper(II) acetate (1 mmol), 3,5-dinitrobenzoic acid (2 mmol) added; ppt. filtered off, washed with water, dried at room temp., further crystals obtained from mother liquor stored at room temp. after a few weeks;

DOI:10.1107/S0108270106025467

upstream raw materials:

[Cu₂(OAc)4(H₂O)2]

3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione

3,5-dinitrobenzoic acid