Furan, 2-[2-(4-nitrophenyl)ethenyl]-

Base Information

• Chemical Name: Furan, 2-[2-(4-nitrophenyl)ethenyl]-
• CAS No.: 20001-01-8
• Molecular Formula: C12H9NO3
• Molecular Weight: 215.208
• Mol file: 20001-01-8.mol

Synonyms:2-[2-(4-Nitrophenyl)vinyl]furan;1-(2'-Furyl)-2-(p-nitrophenyl)-ethylen;2-(4-nitro-styryl)-furan;

Chemical Property of Furan, 2-[2-(4-nitrophenyl)ethenyl]-

Chemical Property:

• Melting Point: 131 °C
• Boiling Point: 313.6±11.0 °C(Predicted)
• PSA: 58.96000
• Density: 1.286±0.06 g/cm3(Predicted)
• LogP: 3.88140

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Furan, 2-[2-(4-nitrophenyl)ethenyl]-

There total 9 articles about Furan, 2-[2-(4-nitrophenyl)ethenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

furfural (98-01-1) + 4-nitrobenzeneacetic acid (104-03-0) → 2-[(1E)-2-(4-nitrophenyl)ethenyl]furan (20001-01-8,51042-57-0)

Guidance literature:

With piperidine; pyridine; at 110 ℃; for 8h;

DOI:10.2174/1570178614666171129161030

Reference yield:

1-bromomethyl-4-nitro-benzene (100-11-8) → C12H9NO3 (20001-01-8)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene

2: sodium ethanolate / ethanol

With sodium ethanolate; In ethanol; benzene;

DOI:10.1016/j.jphotochem.2012.06.009

Reference yield:

furfural (98-01-1) + (p-nitrobenzyl)triphenylphosphonium bromide (2767-70-6) → 2-[(1E)-2-(4-nitrophenyl)ethenyl]furan (20001-01-8,51042-57-0)

Guidance literature:

With sodium methylate; In methanol; for 2h; Heating;

upstream raw materials:

furfural

4-nitrobenzeneacetic acid

ethyl (4-nitrophenyl)pyruvate

(p-nitrobenzyl)triphenylphosphonium bromide

Downstream raw materials:

4-(2ξ-[2]furyl-vinyl)-aniline

2-[2-(4-aminophenyl)ethyl]furan

2-[2-(4-Aminophenyl)ethyl]-5-dimethylaminomethylfuran

2-[2-(4-acetamidophenyl)ethyl]furan