Borinic acid, dicyclohexyl-, (3R,4E)-3-[(4-methoxyphenyl)methoxy]-1-methylene-4-hexenyl ester

Base Information

Chemical Name:Borinic acid, dicyclohexyl-, (3R,4E)-3-[(4-methoxyphenyl)methoxy]-1-methylene-4-hexenyl ester
CAS No.:201355-14-8
Molecular Formula:C₂₇H₄₁BO₃
Molecular Weight:424.432
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Borinic acid, dicyclohexyl-, (3R,4E)-3-[(4-methoxyphenyl)methoxy]-1-methylene-4-hexenyl ester

Chemical Property:

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Technology Process of Borinic acid, dicyclohexyl-, (3R,4E)-3-[(4-methoxyphenyl)methoxy]-1-methylene-4-hexenyl ester

There total 4 articles about Borinic acid, dicyclohexyl-, (3R,4E)-3-[(4-methoxyphenyl)methoxy]-1-methylene-4-hexenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 862474-98-4
(5E)-(4R)-4-p-methoxybenzyloxy-hepta-1,5-diene

: 201355-14-8
C₂₇H₄₁BO₃

Guidance literature:: Multi-step reaction with 2 steps

1: 1.01 g / aq. CuCl; O₂ / PdCl₂ / dimethylformamide / 14 h / 20 °C

2: Et₃N / diethyl ether / 0.5 h / 0 °C

With oxygen; triethylamine; copper(l) chloride; palladium dichloride; In diethyl ether; N,N-dimethyl-formamide; 1: Wacker oxidation;
DOI:10.1039/b504148a

Reference yield:

: 24581-03-1
(5E)-hepta-1,5-dien-4-ol

: 201355-14-8
C₂₇H₄₁BO₃

Guidance literature:: Multi-step reaction with 4 steps

1: 40 percent / diisopropyl L-tartrate; 4 Angstroem molecular sieves; tert-butyl hydroperoxide / Ti(Oi-Pr)4 / CH₂Cl₂; 2,2,4-trimethyl-pentane / 20 h / -20 °C

2: 69 percent / KH; tetrabutylammonium iodide / tetrahydrofuran / 14 h / 20 °C

3: 1.01 g / aq. CuCl; O₂ / PdCl₂ / dimethylformamide / 14 h / 20 °C

4: Et₃N / diethyl ether / 0.5 h / 0 °C

With tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; 4 A molecular sieve; oxygen; tetra-(n-butyl)ammonium iodide; potassium hydride; triethylamine; copper(l) chloride; titanium(IV) isopropylate; palladium dichloride; In tetrahydrofuran; 2,2,4-trimethylpentane; diethyl ether; dichloromethane; N,N-dimethyl-formamide; 1: Sharpless asymmetric epoxidation / 3: Wacker oxidation;
DOI:10.1039/b504148a

Reference yield:

: 89254-01-3
(4R,5E)-(-)-hepta-1,5-dien-4-ol

: 201355-14-8
C₂₇H₄₁BO₃

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / KH; tetrabutylammonium iodide / tetrahydrofuran / 14 h / 20 °C

2: 1.01 g / aq. CuCl; O₂ / PdCl₂ / dimethylformamide / 14 h / 20 °C

3: Et₃N / diethyl ether / 0.5 h / 0 °C

With oxygen; tetra-(n-butyl)ammonium iodide; potassium hydride; triethylamine; copper(l) chloride; palladium dichloride; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; 2: Wacker oxidation;
DOI:10.1039/b504148a