Thiobis(acetohydrazide)

Base Information

• Chemical Name: Thiobis(acetohydrazide)
• CAS No.: 5447-21-2
• Molecular Formula: C4H10N4O2S
• Molecular Weight: 178.215
• Hs Code.: 2930909090
• European Community (EC) Number: 226-663-8
• NSC Number: 16870
• DSSTox Substance ID: DTXSID70202872
• Nikkaji Number: J210.490C
• Mol file: 5447-21-2.mol

Synonyms:Thiobis(acetohydrazide);5447-21-2;2,2'-sulfanediyldiacetohydrazide;EINECS 226-663-8;NSC16870;C4H10N4O2S;SCHEMBL6323330;DTXSID70202872;NSC 16870;NSC-16870;STL583056;2,2'-Thiobis(acetic acid hydrazide);AKOS040894821

Chemical Property of Thiobis(acetohydrazide)

Chemical Property:

• Vapor Pressure: 1.54E-11mmHg at 25°C
• Boiling Point: 535.4°Cat760mmHg
• Flash Point: 277.6°C
• PSA: 135.54000
• Density: 1.394g/cm³
• LogP: -0.11820
• XLogP3: -1.9
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 4
• Exact Mass: 178.05244675
• Heavy Atom Count: 11
• Complexity: 135

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(C(=O)NN)SCC(=O)NN

Technology Process of Thiobis(acetohydrazide)

There total 2 articles about Thiobis(acetohydrazide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl thioglycolate (925-47-3) → bis(hydrazinocarbonylmethyl)sulphide (5447-21-2)

Guidance literature:

With methanol; hydrazine hydrate; acetic acid;

DOI:10.1021/jo01090a614

Reference yield:

→ bis(hydrazinocarbonylmethyl)sulphide (5447-21-2)

Guidance literature:

Diaethylester der Thiodiglycolsaeure, N2H4*H2O;

Reference yield:

bis(hydrazinocarbonylmethyl)sulphide (5447-21-2) + 2-chloro-benzaldehyde (89-98-5) → sulfanediyldi-acetic acid bis-(2-chloro-benzylidenehydrazide) (110059-19-3)

Guidance literature:

With ethanol;

DOI:10.1021/jo01090a614

upstream raw materials:

diethyl thioglycolate

Downstream raw materials:

sulfanediyldiacetic acid bis-trans-cinnamylidene-hydrazide

sulfanediyldi-acetic acid bis-(2-chloro-benzylidenehydrazide)

sulfanediyldi-acetic acid bis-benzylidenehydrazide

sulfanediyldi-acetic acid bis-(4-methoxy-benzylidenehydrazide)