[cobalt(III)(1,2-cyclohexanedione dioxime(-H))2(trimethylphosphine)2](hexafluoroantimonate)

Base Information

• Chemical Name: [cobalt(III)(1,2-cyclohexanedione dioxime(-H))2(trimethylphosphine)2](hexafluoroantimonate)
• CAS No.: 1402168-87-9
• Molecular Formula: C₄₈H₄₈CoN₄O₄P₂*F₆Sb
• Molecular Weight: 1101.61
• Mol file: 1402168-87-9.mol

Synonyms:

Chemical Property of [cobalt(III)(1,2-cyclohexanedione dioxime(-H))2(trimethylphosphine)2](hexafluoroantimonate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [cobalt(III)(1,2-cyclohexanedione dioxime(-H))2(trimethylphosphine)2](hexafluoroantimonate)

There total 1 articles about [cobalt(III)(1,2-cyclohexanedione dioxime(-H))2(trimethylphosphine)2](hexafluoroantimonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

sodium hexafluoroantimonate (16925-25-0) + 1,2-cyclohexanedionedioxime (492-99-9) + cobalt(II) diacetate tetrahydrate (6147-53-1) + triphenylphosphine (603-35-0) → [cobalt(III)(1,2-cyclohexanedione dioxime(-H))2(trimethylphosphine)2](hexafluoroantimonate) (1402168-87-9)

Guidance literature:

In methanol; water; soln. of C6H10N2O2 and PPh3 in MeOH heated to 60°C on water bath;aq. soln. of NaSbF6 and Co salt added dropwise, then heated with reflux for 1 h; soln. filtered, left for slow evapn. at room temp.; elem. anal.;

DOI:10.1134/S1070328412070068

upstream raw materials:

sodium hexafluoroantimonate

1,2-cyclohexanedionedioxime

cobalt(II) diacetate tetrahydrate

triphenylphosphine