2-Propenoic acid, 3-phenyl-, 2-acetyl-3-(phenylmethoxy)phenyl ester, (2E)-

Base Information

Chemical Name:2-Propenoic acid, 3-phenyl-, 2-acetyl-3-(phenylmethoxy)phenyl ester, (2E)-
CAS No.:205308-01-6
Molecular Formula:C24H20O4
Molecular Weight:372.42
Hs Code.:

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Chemical Property of 2-Propenoic acid, 3-phenyl-, 2-acetyl-3-(phenylmethoxy)phenyl ester, (2E)-

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Technology Process of 2-Propenoic acid, 3-phenyl-, 2-acetyl-3-(phenylmethoxy)phenyl ester, (2E)-

There total 1 articles about 2-Propenoic acid, 3-phenyl-, 2-acetyl-3-(phenylmethoxy)phenyl ester, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 4047-24-9
1-[2-(benzyloxy)-6-hydroxyphenyl]ethanone

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 205308-01-6
6'-benzyloxy-2'-(cinnamoyloxy)acetophenone

Guidance literature:: With pyridine; for 2h; Ambient temperature;
DOI:10.1002/jhet.5570350140

Reference yield: 90.9%

: 205308-01-6
6'-benzyloxy-2'-(cinnamoyloxy)acetophenone

: 205308-06-1
1-(6-benzyloxy-2-hydroxyphenyl)-3-hydroxy-5-phenyl-2,4-pentadien-1-one

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 2h;
DOI:10.1002/ejoc.200300468

Reference yield:

: 205308-01-6
6'-benzyloxy-2'-(cinnamoyloxy)acetophenone

: 158264-60-9
(E)-5-benzyloxy-2-styrylchromone

Guidance literature:: Multi-step reaction with 2 steps

1: 90.9 percent / potassium hydroxide / dimethylsulfoxide / 2 h / 20 °C

2: 93.2 percent / p-toluenesulfonic acid monohydrate / dimethylsulfoxide / 90 °C

With potassium hydroxide; toluene-4-sulfonic acid; In dimethyl sulfoxide; 1: Baker-Venkataraman rearrangement;
DOI:10.1002/ejoc.200300468