1H-3-Benzazepine, 2,3,4,5-tetrahydro-7,8-dimethoxy-1-phenyl-

Base Information

Chemical Name:1H-3-Benzazepine, 2,3,4,5-tetrahydro-7,8-dimethoxy-1-phenyl-
CAS No.:20569-49-7
Molecular Formula:C18H21NO2
Molecular Weight:283.37
Hs Code.:
DSSTox Substance ID:DTXSID20441532

Synonyms:20569-49-7;1H-3-Benzazepine, 2,3,4,5-tetrahydro-7,8-dimethoxy-1-phenyl-;SCHEMBL7320752;DTXSID20441532;YCCXFCQLRGMHPB-UHFFFAOYSA-N;7,8-dimethoxy-1-phenyl-2,3,4,5,-tetrahydro-1H-3-benzazepine;7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3 -benzazepine;7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

Suppliers and Price of 1H-3-Benzazepine, 2,3,4,5-tetrahydro-7,8-dimethoxy-1-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-3-Benzazepine, 2,3,4,5-tetrahydro-7,8-dimethoxy-1-phenyl-

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:283.157228913
Heavy Atom Count:21
Complexity:316

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C2C(CNCCC2=C1)C3=CC=CC=C3)OC

Technology Process of 1H-3-Benzazepine, 2,3,4,5-tetrahydro-7,8-dimethoxy-1-phenyl-

There total 5 articles about 1H-3-Benzazepine, 2,3,4,5-tetrahydro-7,8-dimethoxy-1-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 20011-97-6
N-[2-(3,4-dimethoxyphenyl)ethyl]-2-phenyl-2-hydroxyethylamine

: 20569-49-7
7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

Guidance literature:: With sulfuric acid; trifluoroacetic acid; for 3h; Heating;
DOI:10.1021/jm00116a004

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 20569-49-7
7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / tetrahydrofuran / 18 h / Heating

2: 90 percent / 99percent CF₃COOH, 99percent CH₃SO₃H / 18 h / Heating

With methanesulfonic acid; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1021/jm00021a018

Reference yield:

: 96-09-3
styrene oxide

: 20569-49-7
7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / tetrahydrofuran / 18 h / Heating

2: 90 percent / 99percent CF₃COOH, 99percent CH₃SO₃H / 18 h / Heating

With methanesulfonic acid; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1021/jm00021a018