Uridine, 5-ethynyl-, 2',3',5'-triacetate

Base Information

Chemical Name:Uridine, 5-ethynyl-, 2',3',5'-triacetate
CAS No.:209254-94-4
Molecular Formula:C17H18N2O9
Molecular Weight:394.338
Hs Code.:

Synonyms:

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Chemical Property of Uridine, 5-ethynyl-, 2',3',5'-triacetate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Uridine, 5-ethynyl-, 2',3',5'-triacetate

There total 1 articles about Uridine, 5-ethynyl-, 2',3',5'-triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84500-33-4,65499-40-3
2',3',5'-tri-O-acetyl-5-iodouridine

: 209254-94-4
2′,3′,5′-tri-O-acetyl-5-ethynyluridine

Guidance literature:: Multi-step reaction with 2 steps

1: CuI; Et₃N / PdCl₂(PPh₃)2 / dimethylformamide / 20 °C

2: tetra-n-butylammonium fluoride monohydrate / acetonitrile / 20 °C

With copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; acetonitrile; 1: Sonogashira cross-coupling;
DOI:10.1016/j.bmc.2005.06.021

Reference yield: 78.0%

: C₁₄H₈Fe₂N₄O₆S₂

: 209254-94-4
2′,3′,5′-tri-O-acetyl-5-ethynyluridine

: C₃₁H₂₆Fe₂N₆O₁₅S₂

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In N,N-dimethyl-formamide; at 20 ℃; for 30h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.inorgchem.9b02813