Technology Process of 4-Amino-3-methoxybenzamide
There total 7 articles about 4-Amino-3-methoxybenzamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium 10% on activated carbon;
In
ethanol;
at 20 ℃;
for 19h;
- Guidance literature:
-
With
ammonium acetate; N-ethyl-N,N-diisopropylamine; HATU;
In
N,N-dimethyl-formamide;
at 25 ℃;
for 2h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: thionyl chloride; sodium hydroxide / 0.5 h / 80 °C
1.2: 0.5 h / 0 °C
2.1: sodium tetrahydroborate; methanol; nickel(II) chloride hexahydrate / 0 - 23 °C
With
methanol; sodium tetrahydroborate; thionyl chloride; nickel(II) chloride hexahydrate; sodium hydroxide;
