Co(NH(CH₂)2NC(C₆H₅)CH₂CH(CH₃)NH(CH₂)2NC(C₆H₅)CH₂CH(CH₃))Cl₂⁽¹⁺⁾*ClO₄^(1-)={Co(C₂₄H₃₂N₄)Cl₂}ClO₄

Base Information

• Chemical Name: Co(NH(CH₂)2NC(C₆H₅)CH₂CH(CH₃)NH(CH₂)2NC(C₆H₅)CH₂CH(CH₃))Cl₂⁽¹⁺⁾*ClO₄^(1-)={Co(C₂₄H₃₂N₄)Cl₂}ClO₄
• CAS No.: 131680-90-5
• Molecular Formula: C₂₄H₃₂Cl₂CoN₄*ClO₄
• Molecular Weight: 605.895
• Mol file: 131680-90-5.mol

Synonyms:

Chemical Property of Co(NH(CH₂)2NC(C₆H₅)CH₂CH(CH₃)NH(CH₂)2NC(C₆H₅)CH₂CH(CH₃))Cl₂⁽¹⁺⁾*ClO₄^(1-)={Co(C₂₄H₃₂N₄)Cl₂}ClO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Co(NH(CH₂)2NC(C₆H₅)CH₂CH(CH₃)NH(CH₂)2NC(C₆H₅)CH₂CH(CH₃))Cl₂⁽¹⁺⁾*ClO₄^(1-)={Co(C₂₄H₃₂N₄)Cl₂}ClO₄

There total 1 articles about Co(NH(CH₂)2NC(C₆H₅)CH₂CH(CH₃)NH(CH₂)2NC(C₆H₅)CH₂CH(CH₃))Cl₂⁽¹⁺⁾*ClO₄^(1-)={Co(C₂₄H₃₂N₄)Cl₂}ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7,14-dimethyl-5,12-diphenyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene + cobalt(II) diacetate tetrahydrate (6147-53-1) → Co(NH(CH2)2NC(C6H5)CH2CH(CH3)NH(CH2)2NC(C6H5)CH2CH(CH3))Cl2(1+)*ClO4(1-)={Co(C24H32N4)Cl2}ClO4 (131680-90-5)

Guidance literature:

In hydrogenchloride; methanol; perchloric acid; Dissolving of ligand and Co-salt in aq. MeOH, aerating for 24 h, addn. of conc. HCl, heating (green colour appears), addn. of aq. HClO4, concg. until cryst. sets in, filtn. of green complex., suspending in H2O, addn. of Na2CO3, heating, heating in HCl.; Addn. of aq. HClO4, concg., cooling, filtn. of green complex, washing (EtOH, Et2O), drying in vac., elem. anal.;

DOI:10.1039/DT9900003531

upstream raw materials:

cobalt(II) diacetate tetrahydrate