Technology Process of Ethanethiol, 2,2'-[(2-pyridinylmethyl)imino]bis-
There total 1 articles about Ethanethiol, 2,2'-[(2-pyridinylmethyl)imino]bis- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
toluene;
for 30h;
Title compound not separated from byproducts;
Heating;
DOI:10.1246/cl.1998.971
- Guidance literature:
-
With
triethylamine;
In
chloroform;
to a soln. of Re-contg. compd. (0.0986 mmol) in chloroform was added dropwise a soln. of monothiol (0.0986 mmol) and dithiol (0.0986 mmol) in the same solvent; then triethylamine (0.574 mmol) was added; the soln. was stirred and refluxed to 30 min; the soln. was evapd. to dryness; elem. anal.;
DOI:10.1016/S0020-1693(00)00144-4
- Guidance literature:
-
With
triethylamine;
In
chloroform;
to a soln. of Re-contg. compd. (0.0986 mmol) in chloroform was added dropwise a soln. of monothiol (0.0986 mmol) and dithiol (0.0986 mmol) in the same solvent; then triethylamine (0.574 mmol) was added; the soln. was stirred and refluxed to 30 min; the soln. was evapd. to dryness;
DOI:10.1016/S0020-1693(00)00144-4
