Benzenamine, 2,3,4,5,6-pentafluoro-N-sulfinyl-

Base Information

• Chemical Name: Benzenamine, 2,3,4,5,6-pentafluoro-N-sulfinyl-
• CAS No.: 22001-09-8
• Molecular Formula: C6F5NOS
• Molecular Weight: 229.13
• Mol file: 22001-09-8.mol

Synonyms:

Chemical Property of Benzenamine, 2,3,4,5,6-pentafluoro-N-sulfinyl-

Chemical Property:

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Technology Process of Benzenamine, 2,3,4,5,6-pentafluoro-N-sulfinyl-

There total 3 articles about Benzenamine, 2,3,4,5,6-pentafluoro-N-sulfinyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,3,4,5,6-pentafluoroaniline (771-60-8) → N-sulfinylpentafluoroaniline (22001-09-8)

Guidance literature:

With ICF₂CF₂OCF₂CF₂SO₂N=S=O; at 25 ℃; for 8h;

DOI:10.1016/0022-1139(93)03060-Y

Reference yield: 87.0%

thionyl chloride (7719-09-7) + 2,3,4,5,6-pentafluoroaniline (771-60-8) → N-sulfinylpentafluoroaniline (22001-09-8)

Guidance literature:

dropwise addn. of SOCl2 at 20°C to stirred C6F5NH2, reflux 10 h;

DOI:10.1016/0020-1650(68)90010-X

Reference yield:

→ N-sulfinylpentafluoroaniline (22001-09-8)

Guidance literature:

C6F5NH2, SOCl2;

DOI:10.1016/0020-1650(68)90010-X DOI:10.1007/BF00951714

upstream raw materials:

2,3,4,5,6-pentafluoroaniline

thionyl chloride

Downstream raw materials:

C₁₃H₁₃F₅N₂O₂S

C₉H₉F₅N₂O₂S

N,N'-bis(trimethylsilyl)sulfurdiimide

1,3-bis-(pentafluorophenyl)-2-thia-1,3-diazaallene

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