{P(C₆H₁₁)3}2Pd(CH₃OCH₂CCCH₂OCH₃)

Base Information

Chemical Name:{P(C₆H₁₁)3}2Pd(CH₃OCH₂CCCH₂OCH₃)
CAS No.:84181-08-8
Molecular Formula:C₄₂H₇₆O₂P₂Pd
Molecular Weight:781.432
Hs Code.:

{P(C<sub>6</sub>H<sub>11</sub>)3}2Pd(CH<sub>3</sub>OCH<sub>2</sub>CCCH<sub>2</sub>OCH<sub>3</sub>)

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Suppliers and Price of {P(C₆H₁₁)3}2Pd(CH₃OCH₂CCCH₂OCH₃)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {P(C₆H₁₁)3}2Pd(CH₃OCH₂CCCH₂OCH₃)

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Technology Process of {P(C₆H₁₁)3}2Pd(CH₃OCH₂CCCH₂OCH₃)

There total 1 articles about {P(C₆H₁₁)3}2Pd(CH₃OCH₂CCCH₂OCH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33395-48-1
(ethene)bis(tricyclohexylphosphine)palladium⁽⁰⁾

: 16356-02-8
1,4-dimethoxy-2-butyne

: 84181-08-8
{P(C₆H₁₁)3}2Pd(CH₃OCH₂CCCH₂OCH₃)

Guidance literature:: In tetrahydrofuran; toluene; byproducts: CH2CH2; (Ar); equimolar amts.; dissolving the Pd-complex at -30°C in toluene; dropwise addn. of the acetylene compound soln. (in THF) with stirring at this temp.; stirring for 45 min; filtration over silica gel; addn. of hexane to the filtrate; filtation over silica gel; crystn. at -10°C (several hours); recrystn. from THF/hexane or ether/THF; elem. anal.;