(C₂H₅)3Sn(CH₂SC₆H₅)

Base Information

• Chemical Name: (C₂H₅)3Sn(CH₂SC₆H₅)
• CAS No.: 83991-17-7
• Molecular Formula: C₁₃H₂₂SSn
• Molecular Weight: 329.094
• Mol file: 83991-17-7.mol

Synonyms:

Chemical Property of (C₂H₅)3Sn(CH₂SC₆H₅)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (C₂H₅)3Sn(CH₂SC₆H₅)

There total 1 articles about (C₂H₅)3Sn(CH₂SC₆H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chlorotriethylstannane (994-31-0) + (phenylthio)methyllithium (13307-75-0) → (C2H5)3Sn(CH2SC6H5) (83991-17-7)

Guidance literature:

In not given; to stirred soln. of C6H5SCH2Li in Et2O or THF dropwise added soln. of Et3SnCl in Et2O or THF at -10 °C, warmed to room temp., stirred for 1 h; cooled to -50 °C, dropwise added aq. NH4Cl, washed with H2O, dried over Na2SO4, distd. in vac.;

DOI:10.1016/0022-328X(82)80003-X

upstream raw materials:

chlorotriethylstannane

(phenylthio)methyllithium