2-Propanol, 1-[(4-methoxyphenyl)methoxy]-3-(triphenylmethoxy)-, (2S)-

Base Information

Chemical Name:2-Propanol, 1-[(4-methoxyphenyl)methoxy]-3-(triphenylmethoxy)-, (2S)-
CAS No.:220641-23-6
Molecular Formula:C30H30O4
Molecular Weight:454.566
Hs Code.:
Mol file:220641-23-6.mol

Synonyms:2-Propanol,1-[(4-methoxyphenyl)methoxy]-3-(triphenylmethoxy)-,(2S);

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Propanol, 1-[(4-methoxyphenyl)methoxy]-3-(triphenylmethoxy)-, (2S)-

Chemical Property:

PSA：47.92000
LogP:5.58140

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Propanol, 1-[(4-methoxyphenyl)methoxy]-3-(triphenylmethoxy)-, (2S)-

There total 3 articles about 2-Propanol, 1-[(4-methoxyphenyl)methoxy]-3-(triphenylmethoxy)-, (2S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 76-83-5
trityl chloride

: 109786-74-5
(R)-3-(4-methoxybenzyloxy)propane-1,2-diol

: 220641-23-6
1-O-(triphenylmethyl)-3-O-(4'-methoxybenzyl)-sn-glycerol

Guidance literature:: With pyridine; dmap; In dichloromethane; Ambient temperature;
DOI:10.1021/ja982837o

Reference yield:

: 109786-73-4
(S)-4-[(4-methoxybenzyloxy)methyl]-2,2-dimethyl-1,3-dioxolane

: 220641-23-6
1-O-(triphenylmethyl)-3-O-(4'-methoxybenzyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: 24.5 g / p-TsOH / methanol / 2 h

2: pyridine; DMAP / CH₂Cl₂

With pyridine; dmap; toluene-4-sulfonic acid; In methanol; dichloromethane;
DOI:10.1021/jm049006f

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 220641-23-6
1-O-(triphenylmethyl)-3-O-(4'-methoxybenzyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / tetrahydrofuran; dimethylformamide / 1 h

1.2: Bu₄NI / tetrahydrofuran; dimethylformamide

2.1: 24.5 g / p-TsOH / methanol / 2 h

3.1: pyridine; DMAP / CH₂Cl₂

With pyridine; dmap; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm049006f